iridium(I) d,l-2,2'-bis[[o-(diphenylphosphino)benzylidene]amino]-6,6'-dimethylbiphenyl complex tetraphenylborate

Base Information

Chemical Name:iridium(I) d,l-2,2'-bis[[o-(diphenylphosphino)benzylidene]amino]-6,6'-dimethylbiphenyl complex tetraphenylborate
CAS No.:93565-26-5
Molecular Formula:C₂₄H₂₀B*C₅₂H₄₂IrN₂P₂
Molecular Weight:1268.32
Hs Code.:

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Chemical Property of iridium(I) d,l-2,2'-bis[[o-(diphenylphosphino)benzylidene]amino]-6,6'-dimethylbiphenyl complex tetraphenylborate

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Technology Process of iridium(I) d,l-2,2'-bis[[o-(diphenylphosphino)benzylidene]amino]-6,6'-dimethylbiphenyl complex tetraphenylborate

There total 1 articles about iridium(I) d,l-2,2'-bis[[o-(diphenylphosphino)benzylidene]amino]-6,6'-dimethylbiphenyl complex tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 21414-18-6,15695-36-0,18433-33-5
(PPh₃)2Ir(dinitrogen)Cl

: 93565-30-1,347164-00-5
d,l-2,2'-bis[[o-(diphenylphosphino)benzylidene]amino]-6,6'-dimethylbiphenyl

: 143-66-8
sodium tetraphenyl borate

: 93565-26-5
iridium(I) d,l-2,2'-bis[[o-(diphenylphosphino)benzylidene]amino]-6,6'-dimethylbiphenyl complex tetraphenylborate

Guidance literature:: In dichloromethane; adding of ice-cold soln. of Ir complex to a cold soln. of ligand; stirring at 0°C for 1 h, mixing with a soln. of NaBPh4 in MeOH, stirring at 0°C for 20 min; evapn., filtration, washing with MeOH and Et2O, drying in vac.; elem. anal.;