4-METHOXY-3-[(4-METHYLBENZYL)OXY]BENZALDEHYDE

Base Information

• Chemical Name: 4-METHOXY-3-[(4-METHYLBENZYL)OXY]BENZALDEHYDE
• CAS No.: 351066-34-7
• Molecular Formula: C₁₆H₁₆O₃
• Molecular Weight: 256.301
• Hs Code.: 2912499000
• Mol file: 351066-34-7.mol

Synonyms:

Chemical Property of 4-METHOXY-3-[(4-METHYLBENZYL)OXY]BENZALDEHYDE

Chemical Property:

• Vapor Pressure: 7.72E-07mmHg at 25°C
• Boiling Point: 407.1oC at 760 mmHg
• Flash Point: 191.7oC
• PSA: 35.53000
• Density: 1.133g/cm3
• LogP: 3.39510

Purity/Quality:

98%min ^*data from raw suppliers

4-Methoxy-3-[(4-methylbenzyl)oxy]benzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-METHOXY-3-[(4-METHYLBENZYL)OXY]BENZALDEHYDE

There total 1 articles about 4-METHOXY-3-[(4-METHYLBENZYL)OXY]BENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isovanillin (621-59-0) + 4-Methylbenzyl chloride (104-82-5) → C16H16O3 (351066-34-7)

Guidance literature:

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 90 ℃;

DOI:10.1016/j.cclet.2010.06.023

Reference yield:

3-Morpholin-4-yl-propionitrile (4542-47-6) + C16H16O3 (351066-34-7) → C23H26N2O3

Guidance literature:

With sodium methylate; In dimethyl sulfoxide; at 75 ℃;

DOI:10.1016/j.cclet.2010.06.023

Reference yield:

C16H16O3 (351066-34-7) → C25H24N2O2 (1256645-28-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium methylate / dimethyl sulfoxide / 75 °C

2: isopropyl alcohol / Reflux

With sodium methylate; In dimethyl sulfoxide; isopropyl alcohol;

DOI:10.1016/j.cclet.2010.06.023

upstream raw materials:

isovanillin

4-Methylbenzyl chloride

Downstream raw materials:

C₂₅H₂₄N₂O₂

C₂₀H₂₂N₄O₂

Refernces