4-Oxo-2,2,6,6-tetramethylpiperidine-D16-1-oxyl

Base Information

Chemical Name:4-Oxo-2,2,6,6-tetramethylpiperidine-D16-1-oxyl
CAS No.:36763-53-8
Molecular Formula:C₉H₁₆NO₂
Molecular Weight:186.104
Hs Code.:
European Community (EC) Number:695-498-5
Nikkaji Number:J582.888K
Mol file:36763-53-8.mol

Synonyms:36763-53-8;4-Oxo-TEMPO-d16, free radical;4-OXO-2,2,6,6-TETRAMETHYLPIPERIDINE-D16-1-OXYL;CID 16213282;DTXSID00583843;4-Oxo-TEMPO-d16, free radical, for ESR-spectroscopy, 97 atom % D;{2,2,6,6-Tetrakis[(~2~H_3_)methyl]-4-oxo(~2~H_4_)piperidin-1-yl}oxidanyl

Suppliers and Price of 4-Oxo-2,2,6,6-tetramethylpiperidine-D16-1-oxyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
4-Oxo-TEMPO-d16, free radical for ESR-spectroscopy, 97 atom % D
500mg
$ 1260.00

Medical Isotopes, Inc.
4-Oxo-2,2,6,6-tetramethylpiperidine-d16-1-oxyl
0.1 g
$ 810.00

American Custom Chemicals Corporation
4-OXO-2,2,6,6-TETRAMETHYLPIPERIDINE-D16-1-OXYL 95.00%
5MG
$ 504.42

Total 10 raw suppliers

Chemical Property of 4-Oxo-2,2,6,6-tetramethylpiperidine-D16-1-oxyl

Chemical Property:

Melting Point:35 °C(lit.)
PSA：20.31000
LogP:1.49190
Storage Temp.:0-6°C
XLogP3:0.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:186.218531688
Heavy Atom Count:12
Complexity:189

Purity/Quality:

99%, ^*data from raw suppliers

4-Oxo-TEMPO-d16, free radical for ESR-spectroscopy, 97 atom % D ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CC1(CC(=O)CC(N1[O])(C)C)C
Isomeric SMILES:[2H]C1(C(=O)C(C(N(C1(C([2H])([2H])[2H])C([2H])([2H])[2H])[O])(C([2H])([2H])[2H])C([2H])([2H])[2H])([2H])[2H])[2H]
Uses 4-Oxo-2,2,6,6-tetramethylpiperidine-d16-1-oxyl (CAS# 36763-53-8) is a useful isotopically labeled research compound.

Technology Process of 4-Oxo-2,2,6,6-tetramethylpiperidine-D16-1-oxyl

There total 3 articles about 4-Oxo-2,2,6,6-tetramethylpiperidine-D16-1-oxyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.1%

: 73322-03-9
1H-perdeutero-2,2,6,6-tetramethyl-4-piperidone

: 36763-53-8
2,2,6,6-tetramethyl-4-piperidone-N-oxyl-d16

Guidance literature:: With sodium tungstate (VI) dihydrate; dihydrogen peroxide; In water; at 5 - 25 ℃;
DOI:10.1002/ardp.200800053

Reference yield:

: 666-52-4
[⁽²⁾H₆]acetone

: 36763-53-8
2,2,6,6-tetramethyl-4-piperidone-N-oxyl-d16

Guidance literature:: With ammonia-d3; calcium chloride; Yield given. Multistep reaction; 1.) D₂O, 203 K to RT, 36 h then RT, 7 d;
DOI:10.1021/j150655a019