Benzaldehyde, 2-(diphenylphosphino)-5-[(4-ethenylphenyl)methoxy]-

Base Information

Chemical Name:Benzaldehyde, 2-(diphenylphosphino)-5-[(4-ethenylphenyl)methoxy]-
CAS No.:351418-53-6
Molecular Formula:C28H23O2P
Molecular Weight:422.45500
Hs Code.:
Mol file:351418-53-6.mol

Synonyms:2-Diphenylphosphanyl-5-(4-vinyl-benzyloxy)-benzaldehyde;

Suppliers and Price of Benzaldehyde, 2-(diphenylphosphino)-5-[(4-ethenylphenyl)methoxy]-

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Chemical Property of Benzaldehyde, 2-(diphenylphosphino)-5-[(4-ethenylphenyl)methoxy]-

Chemical Property:

PSA：39.89000
LogP:5.47930

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Benzaldehyde, 2-(diphenylphosphino)-5-[(4-ethenylphenyl)methoxy]-

There total 3 articles about Benzaldehyde, 2-(diphenylphosphino)-5-[(4-ethenylphenyl)methoxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2973-80-0
2-bromo-5-hydroxybenzaldehyde

: 351418-53-6
2-diphenylphosphanyl-5-(4-vinylbenzyloxy)benzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / imidazole / dimethylformamide / 1 h / 20 °C

2: Et₃N / Pd(PPh₃)4 / toluene / 2 h / Heating

3: 81 percent / KF; aq. HBr / dimethylformamide / 1 h / 20 °C

4: 56 percent / NaH / dimethylformamide / 12 h / 20 °C

With 1H-imidazole; potassium fluoride; hydrogen bromide; sodium hydride; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; toluene;
DOI:10.1002/1615-4169(200108)343:6/7<711::aid-adsc711>3.3.co;2-t

Reference yield:

: 351418-50-3
2-bromo-5-(tert-butyldimethylsilanyloxy)benzaldehyde

: 351418-53-6
2-diphenylphosphanyl-5-(4-vinylbenzyloxy)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / Pd(PPh₃)4 / toluene / 2 h / Heating

2: 81 percent / KF; aq. HBr / dimethylformamide / 1 h / 20 °C

3: 56 percent / NaH / dimethylformamide / 12 h / 20 °C

With potassium fluoride; hydrogen bromide; sodium hydride; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; toluene;
DOI:10.1002/1615-4169(200108)343:6/7<711::aid-adsc711>3.3.co;2-t

Reference yield:

: 351418-51-4
5-(tert-butyldimethylsilanyloxy)-2-diphenylphosphanylbenzaldehyde

: 351418-53-6
2-diphenylphosphanyl-5-(4-vinylbenzyloxy)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / KF; aq. HBr / dimethylformamide / 1 h / 20 °C

2: 56 percent / NaH / dimethylformamide / 12 h / 20 °C

With potassium fluoride; hydrogen bromide; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1002/1615-4169(200108)343:6/7<711::aid-adsc711>3.3.co;2-t