5,6-Dichloro-3-iminoisoindolin-1-one

Base Information

Chemical Name:5,6-Dichloro-3-iminoisoindolin-1-one
CAS No.:35190-38-6
Molecular Formula:C₈H₄Cl₂N₂O
Molecular Weight:215.039
Hs Code.:
DSSTox Substance ID:DTXSID90438919
Nikkaji Number:J2.723.237J,J26.841K
Mol file:35190-38-6.mol

Synonyms:35190-38-6;5,6-dichloro-3-iminoisoindolin-1-one;5,6-dichloro-3-imino-2,3-dihydro-1H-isoindol-1-one;3-amino-5,6-dichloroisoindol-1-one;1H-Isoindol-1-one, 3-amino-5,6-dichloro-;SCHEMBL3143957;DTXSID90438919;(5,6-Dichloro-1-oxoisoindoline-2-ide)-3-ylideneiminium

Suppliers and Price of 5,6-Dichloro-3-iminoisoindolin-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5,6-dichloro-3-imino-2,3-dihydro-1H-isoindol-1-one
50mg
$ 350.00

TRC
5,6-dichloro-3-imino-2,3-dihydro-1H-isoindol-1-one
10mg
$ 90.00

TRC
5,6-dichloro-3-imino-2,3-dihydro-1H-isoindol-1-one
5mg
$ 65.00

Total 1 raw suppliers

Chemical Property of 5,6-Dichloro-3-iminoisoindolin-1-one

Chemical Property:

Melting Point:330-335 °C (decomp)
Boiling Point:428.5±55.0 °C(Predicted)
PSA：56.44000
Density:1.76±0.1 g/cm3(Predicted)
LogP:2.17230
XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:213.9700681
Heavy Atom Count:13
Complexity:279

Purity/Quality:: 5,6-dichloro-3-imino-2,3-dihydro-1H-isoindol-1-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C2C(=CC(=C1Cl)Cl)C(=O)N=C2N

Technology Process of 5,6-Dichloro-3-iminoisoindolin-1-one

There total 3 articles about 5,6-Dichloro-3-iminoisoindolin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 139152-08-2
4,5-dichlorophthalonitrile

: 35190-38-6
5,6-dichloro-3-iminoisoindolin-1-one

Guidance literature:: With N-ethyl-N-hydroxy-ethanamine; In chloroform; for 4h; Reflux;
DOI:10.1002/adsc.200700261

Reference yield:

: 71969-20-5
2-cyano-4,5-dichlorobenzoic acid methyl ester

: 35190-38-6
5,6-dichloro-3-iminoisoindolin-1-one

Guidance literature:: With ammonia; In methanol; for 72h; Ambient temperature;
DOI:10.1021/jm00102a016

Reference yield:

: 110568-92-8
2-carbamoyl-4,5-dichlorobenzoic acid

: 35190-38-6
5,6-dichloro-3-iminoisoindolin-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / triethylamine / CH₂Cl₂ / Ambient temperature

2: ammonia gas / methanol / 72 h / Ambient temperature

With ammonia; triethylamine; In methanol; dichloromethane;
DOI:10.1021/jm00102a016