(Bis(dimethylamino)methylene)dimethylthiourea

Base Information

• Chemical Name: (Bis(dimethylamino)methylene)dimethylthiourea
• CAS No.: 34619-07-3
• Molecular Formula: C8H18 N4 S
• Molecular Weight: 202.324
• Hs Code.: 2930909090
• European Community (EC) Number: 252-114-7
• UNII: 3C2DBP7YQP
• DSSTox Substance ID: DTXSID20188192
• Nikkaji Number: J250.931H
• Mol file: 34619-07-3.mol

Synonyms:(Bis(dimethylamino)methylene)dimethylthiourea;3C2DBP7YQP;34619-07-3;EINECS 252-114-7;UNII-3C2DBP7YQP;DTXSID20188192;N-[Bis(dimethylamino)methylene]-N',N'-dimethylthiourea;N'-(BIS(DIMETHYLAMINO)METHYLENE)-N,N-DIMETHYLTHIOUREA;THIOUREA, N'-(BIS(DIMETHYLAMINO)METHYLENE)-N,N-DIMETHYL-

Chemical Property of (Bis(dimethylamino)methylene)dimethylthiourea

Chemical Property:

• Vapor Pressure: 0.0281mmHg at 25°C
• Boiling Point: 245.8°Cat760mmHg
• Flash Point: 102.5°C
• PSA: 54.17000
• Density: 1g/cm³
• LogP: 0.31210
• XLogP3: 0.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 202.12521776
• Heavy Atom Count: 13
• Complexity: 198

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C(=NC(=S)N(C)C)N(C)C

Technology Process of (Bis(dimethylamino)methylene)dimethylthiourea

There total 1 articles about (Bis(dimethylamino)methylene)dimethylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N--N',N'-dimethylthioharnstoff (34619-07-3)

Guidance literature:

<(CH3)2N>2C=NH, (CH3)2NCSCl;

Reference yield: 91.0%

N--N',N'-dimethylthioharnstoff (34619-07-3) + allyl bromide (106-95-6) → 1-Allylthio-3,3-bis-N,N-dimethyl-2-azapropeniminium-bromid

Guidance literature:

In diethyl ether; acetone; for 3h; Ambient temperature;

DOI:10.1055/s-1981-29560

Reference yield:

N--N',N'-dimethylthioharnstoff (34619-07-3) → 2,4-Bis-1,3-thiazol-5-(N-phenylpropenthioamid) (79577-03-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 91 percent / acetone; diethyl ether / 3 h / Ambient temperature

2: 85 percent / NaH / tetrahydrofuran / 1.) 24h, room temp., 2.) 1h, reflux

3: 52 percent / toluene / 18 h / Heating

With sodium hydride; In tetrahydrofuran; diethyl ether; acetone; toluene;

DOI:10.1055/s-1981-29560

Downstream raw materials:

2,4-Bis-1,3-thiazol-5-(N-phenylpropenthioamid)