Diazenecarboxamide, 2-(4-chlorophenyl)-N-phenyl-

Base Information

• Chemical Name: Diazenecarboxamide, 2-(4-chlorophenyl)-N-phenyl-
• CAS No.: 35524-36-8
• Molecular Formula: C13H10ClN3O
• Molecular Weight: 259.695
• Mol file: 35524-36-8.mol

Synonyms:

Chemical Property of Diazenecarboxamide, 2-(4-chlorophenyl)-N-phenyl-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Diazenecarboxamide, 2-(4-chlorophenyl)-N-phenyl-

There total 7 articles about Diazenecarboxamide, 2-(4-chlorophenyl)-N-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1-(4-chlorophenyl)-4-phenylsemicarbazide (14577-03-8) → 2-(4-chlorophenyl)-N-phenyldiazenecarboxamide (35524-36-8)

Guidance literature:

With ammonium cerium (IV) nitrate; In methanol; at 20 ℃;

DOI:10.1016/j.ejmech.2013.12.057

Reference yield:

phenyl isocyanate (103-71-9) + N-4-chlorophenylhydrazine (1073-69-4) → 2-(4-chlorophenyl)-N-phenyldiazenecarboxamide (35524-36-8)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 20 °C

2: ammonium cerium (IV) nitrate / methanol / 20 °C

With ammonium cerium (IV) nitrate; triethylamine; In methanol; dichloromethane;

DOI:10.1016/j.ejmech.2013.12.057

Reference yield:

C14H13ClN4O2 (62656-87-5) → 2-(4-chlorophenyl)-N-phenyldiazenecarboxamide (35524-36-8)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH, MeOH

2: HgO, KOH

With methanol; potassium hydroxide; mercury(II) oxide;

upstream raw materials:

1-(4-chlorophenyl)-4-phenylsemicarbazide

C₁₄H₁₃ClN₄O₂

phenyl isocyanate

N-4-chlorophenylhydrazine

Refernces