3,5-Dimethyl-4-nitrobenzoyl chloride

Base Information

Chemical Name:3,5-Dimethyl-4-nitrobenzoyl chloride
CAS No.:3558-73-4
Molecular Formula:C9H8ClNO3
Molecular Weight:213.62
Hs Code.:
DSSTox Substance ID:DTXSID10490675
Wikidata:Q82334594
Mol file:3558-73-4.mol

Synonyms:3,5-dimethyl-4-nitrobenzoyl chloride;3558-73-4;SCHEMBL1811071;DTXSID10490675;XDNZLOFKKSKKTJ-UHFFFAOYSA-N

Suppliers and Price of 3,5-Dimethyl-4-nitrobenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3,5-Dimethyl-4-nitrobenzoyl chloride

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:213.0192708
Heavy Atom Count:14
Complexity:239

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1[N+](=O)[O-])C)C(=O)Cl

Technology Process of 3,5-Dimethyl-4-nitrobenzoyl chloride

There total 3 articles about 3,5-Dimethyl-4-nitrobenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 3095-38-3
3,5-dimethyl-4-nitrobenzoic acid

: 3558-73-4
3,5-dimethyl-4-nitrobenzoic acid chloride

Guidance literature:: With thionyl chloride; for 3h; Heating;
DOI:10.1021/jo00183a024

Reference yield:

: 603-71-4,34505-32-3,82795-90-2
nitromesitylene

: 3558-73-4
3,5-dimethyl-4-nitrobenzoic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 14 percent / CrO₃; H₂SO₄ / acetic acid; H₂O

2: SOCl₂

With chromium(VI) oxide; thionyl chloride; sulfuric acid; In water; acetic acid;
DOI:10.1246/cl.2002.1166