N-(p-methoxyphenyl)acetimidoyl chloride

Base Information

Chemical Name:N-(p-methoxyphenyl)acetimidoyl chloride
CAS No.:3583-56-0
Molecular Formula:C9H10ClNO
Molecular Weight:183.637
Hs Code.:
DSSTox Substance ID:DTXSID901276845

Synonyms:N-(p-methoxyphenyl)acetimidoyl chloride;DTXSID901276845;N-(4-Methoxyphenyl)ethanimidoyl chloride;3583-56-0

Suppliers and Price of N-(p-methoxyphenyl)acetimidoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of N-(p-methoxyphenyl)acetimidoyl chloride

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:183.0450916
Heavy Atom Count:12
Complexity:162

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=NC1=CC=C(C=C1)OC)Cl

Technology Process of N-(p-methoxyphenyl)acetimidoyl chloride

There total 1 articles about N-(p-methoxyphenyl)acetimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51-66-1
4-methoxyacetanilide

: 3583-56-0
N-(4-Methoxy-phenyl)-acetimidoyl chloride

Guidance literature:: With 2,6-dimethylpyridine; oxalyl dichloride; In dichloromethane; at 0 ℃; for 0.666667h;
DOI:10.1080/00397910600638994

Reference yield:

: 75553-23-0,106262-48-0,39520-63-3
5-phenylpenta-2-en-1-ol

: 3583-56-0
N-(4-Methoxy-phenyl)-acetimidoyl chloride

: C₂₀H₂₃NO₂

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 2h;
DOI:10.1039/c4cy01749h

Reference yield:

: 3583-56-0
N-(4-Methoxy-phenyl)-acetimidoyl chloride

: 562870-93-3
N-(4-methoxyphenyl)-N-[1-(2-phenylethyl)prop-2-en-1-yl]amine

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -78 - 20 °C

2: silver(I) 4-methylbenzenesulfonate; 4C₂₇H₂₂N₂O₂S^(2-)*4Pd⁽²⁺⁾*4Cl^(1-)*2Fe⁽²⁺⁾; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / chloroform / 72 h / 25 °C

3: Li⁽¹⁺⁾*H⁽¹⁺⁾*C₆H₁₅B / tetrahydrofuran / 2 h / 0 - 25 °C

With Li⁽¹⁺⁾*H⁽¹⁺⁾*C₆H₁₅B; 4C₂₇H₂₂N₂O₂S^(2-)*4Pd⁽²⁺⁾*4Cl^(1-)*2Fe⁽²⁺⁾; silver(I) 4-methylbenzenesulfonate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; lithium hexamethyldisilazane; In tetrahydrofuran; chloroform;
DOI:10.1039/c4cy01749h