N-phenylbutanethioamide

Base Information

Chemical Name:N-phenylbutanethioamide
CAS No.:18051-60-0
Molecular Formula:C10H13NS
Molecular Weight:179.286
Hs Code.:
DSSTox Substance ID:DTXSID30401788
Nikkaji Number:J1.442.280C
NSC Number:97543
Mol file:18051-60-0.mol

Synonyms:18051-60-0;N-phenylbutanethioamide;NSC97543;SCHEMBL1816930;DTXSID30401788;NSC-97543

Suppliers and Price of N-phenylbutanethioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of N-phenylbutanethioamide

Chemical Property:

Vapor Pressure:0.0115mmHg at 25°C
Boiling Point:261.6°C at 760 mmHg
Flash Point:112°C
Density:1.097g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:179.07687059
Heavy Atom Count:12
Complexity:139

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC(=S)NC1=CC=CC=C1

Technology Process of N-phenylbutanethioamide

There total 6 articles about N-phenylbutanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.8%

: 62-53-3
aniline

: 317818-13-6
butyryl 2-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl)sulfide

: 18051-60-0
N-phenylthiobutyramide

Guidance literature:: butyryl 2-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl)sulfide; With 5,5-dimethyl-2-thiolo-2-thiono-1,3,2-dioxaphosphorinane; In benzene; for 3h; Heating;

aniline; With triethylamine; In benzene; Further stages.;
DOI:10.1039/b201233b

Reference yield: 89.0%

: 1129-50-6
N-phenylbutyramide

: 18051-60-0
N-phenylthiobutyramide

Guidance literature:: In toluene;

Reference yield: 30.0%

: 112342-79-7
Butyrophenonoxim (anti-Phenyl)

: 18051-60-0
N-phenylthiobutyramide

Guidance literature:: (E)-1-phenylbutan-1-one oxime; With tetrachloromethane; triphenylphosphine; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

With sodium hydrosulfide monohydrate; at 20 ℃; for 12h;
DOI:10.1016/j.cclet.2021.10.020