Phosphonic acid, [[2-[2-amino-6-[(4-hydroxyphenyl)thio]-9H-purin-9-yl]ethoxy]methyl]-, bis(2,2,2-trifluoroethyl) ester

Base Information

Chemical Name:Phosphonic acid, [[2-[2-amino-6-[(4-hydroxyphenyl)thio]-9H-purin-9-yl]ethoxy]methyl]-, bis(2,2,2-trifluoroethyl) ester
CAS No.:358975-84-5
Molecular Formula:C18H18F6N5O5PS
Molecular Weight:561.402
Hs Code.:
Mol file:358975-84-5.mol

Synonyms:

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Chemical Property of Phosphonic acid, [[2-[2-amino-6-[(4-hydroxyphenyl)thio]-9H-purin-9-yl]ethoxy]methyl]-, bis(2,2,2-trifluoroethyl) ester

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Technology Process of Phosphonic acid, [[2-[2-amino-6-[(4-hydroxyphenyl)thio]-9H-purin-9-yl]ethoxy]methyl]-, bis(2,2,2-trifluoroethyl) ester

There total 2 articles about Phosphonic acid, [[2-[2-amino-6-[(4-hydroxyphenyl)thio]-9H-purin-9-yl]ethoxy]methyl]-, bis(2,2,2-trifluoroethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186345-40-4
bis(2,2,2-trifluoroethyl) [(2-chloroethoxy)methyl]phosphonate

: 358975-84-5
2-amino-6-(4-hydroxyphenylthio)-9-[2-(phosphonomethoxy)ethyl]purine bis(2,2,2-trifluoroethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 80 percent / NaI

2.1: DBU

2.2: 33 percent / dimethylformamide

3.1: 55 percent / pyridine / dimethylformamide

With pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.10.007

Reference yield:

: 186345-41-5
bis(trifluoroethyl) (2-iodoethoxymethyl)phosphonate

: 358975-84-5
2-amino-6-(4-hydroxyphenylthio)-9-[2-(phosphonomethoxy)ethyl]purine bis(2,2,2-trifluoroethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: DBU

1.2: 33 percent / dimethylformamide

2.1: 55 percent / pyridine / dimethylformamide

With pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.10.007