2,3,4,5-tetrahydro-1H-3-benzazepin-7-ol

Base Information

Chemical Name:2,3,4,5-tetrahydro-1H-3-benzazepin-7-ol
CAS No.:36133-00-3
Molecular Formula:C10H13NO
Molecular Weight:163.219
Hs Code.:2933990090
DSSTox Substance ID:DTXSID30605567
Wikidata:Q82503868
Mol file:36133-00-3.mol

Synonyms:36133-00-3;2,3,4,5-tetrahydro-1H-3-benzazepin-7-ol;2,3,4,5-Tetrahydro-1H-benzo[d]azepin-7-ol;1H-3-Benzazepin-7-ol, 2,3,4,5-tetrahydro-;SCHEMBL4030395;DTXSID30605567;MHMRQHMKGYLQKH-UHFFFAOYSA-N;MFCD09802231;AKOS006230519;CCG-355948;SB17683;BS-13689;SY272608;EN300-51442;P20370;AB00996115-01

Suppliers and Price of 2,3,4,5-tetrahydro-1H-3-benzazepin-7-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2,3,4,5-Tetrahydro-1H-benzo[d]azepin-7-ol 95+%
1g
$ 780.00

American Custom Chemicals Corporation
2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPIN-7-OL 95.00%
1G
$ 1143.61

American Custom Chemicals Corporation
2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPIN-7-OL 95.00%
5G
$ 2392.33

American Custom Chemicals Corporation
2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPIN-7-OL 95.00%
2.5G
$ 1771.13

Alichem
2,3,4,5-Tetrahydro-1H-benzo[d]azepin-7-ol
1g
$ 646.84

Abosyn
2,3,4,5-Tetrahydro-1H-benzo[d]azepin-7-ol 95%
5g
$ 1600.00

Abosyn
2,3,4,5-Tetrahydro-1H-benzo[d]azepin-7-ol 95%
1g
$ 480.00

Total 12 raw suppliers

Chemical Property of 2,3,4,5-tetrahydro-1H-3-benzazepin-7-ol

Chemical Property:

PSA：32.26000
LogP:1.40920
Storage Temp.:2-8°C
XLogP3:1.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:163.099714038
Heavy Atom Count:12
Complexity:149

Purity/Quality:

97% ^*data from raw suppliers

2,3,4,5-Tetrahydro-1H-benzo[d]azepin-7-ol 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CNCCC2=C1C=CC(=C2)O

Technology Process of 2,3,4,5-tetrahydro-1H-3-benzazepin-7-ol

There total 7 articles about 2,3,4,5-tetrahydro-1H-3-benzazepin-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 50351-80-9
7-methoxy-2,3,4,5-tetrahydro-1H-benz[d]azepine

: 36133-00-3
2,3,4,5-tetrahydro-1H-benzo[d]azepin-7-ol

Guidance literature:: With hydrogen bromide; for 3h; Heating;
DOI:10.1016/S0960-894X(00)00505-9

Reference yield:

: 4133-34-0
7-methoxyl-2-tetralone

: 36133-00-3
2,3,4,5-tetrahydro-1H-benzo[d]azepin-7-ol

: 247133-23-9
2,3,4,5-tetrahydro-1H-benzo[c]azepin-8-ol

Guidance literature:: 7-methoxyl-2-tetralone; With sodium azide; sulfuric acid;

With borane; In tetrahydrofuran; for 18h; Reflux;

With hydrogen bromide; In water;
DOI:10.1016/j.bmcl.2010.10.083

Reference yield:

: 1229622-03-0
7-methoxy-2,3,4,5-tetrahydro-1H-benzo[d]azepin-1-ol

: 36133-00-3
2,3,4,5-tetrahydro-1H-benzo[d]azepin-7-ol

Guidance literature:: Multi-step reaction with 2 steps

1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 4 h / 20 °C

2: hydrogen bromide / 5 h / Reflux

With triethylsilane; boron trifluoride diethyl etherate; hydrogen bromide; In dichloromethane;
DOI:10.1016/j.ejmech.2019.05.034