Benzenesulfonic acid, 4-[(2-pyridinylmethylene)amino]-, sodium salt

Base Information

Chemical Name:Benzenesulfonic acid, 4-[(2-pyridinylmethylene)amino]-, sodium salt
CAS No.:361348-23-4
Molecular Formula:C₁₂H₉N₂O₃S*Na
Molecular Weight:284.271
Hs Code.:

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Chemical Property of Benzenesulfonic acid, 4-[(2-pyridinylmethylene)amino]-, sodium salt

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Technology Process of Benzenesulfonic acid, 4-[(2-pyridinylmethylene)amino]-, sodium salt

There total 1 articles about Benzenesulfonic acid, 4-[(2-pyridinylmethylene)amino]-, sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62-53-3
aniline

: 361348-23-4
4-[(2-pyridinylmethylene)amino]benzenesulfonic acid sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; sodium hydroxide / 180 - 190 °C

2: toluene

With sulfuric acid; sodium hydroxide; In toluene;
DOI:10.1007/s11243-011-9564-1

Reference yield: 88.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 361348-23-4
4-[(2-pyridinylmethylene)amino]benzenesulfonic acid sodium salt

: 656230-03-4
[PdCl₂(NC₅H₄CH=NC₆H₄-4-SO₃Na)]

Guidance literature:: In methanol; (N2); standard Schlenk technique; methanol was added by syringe to mixt.of Pd complex and ligand; soln. was sealed and stirred for 20 h; filtered; washed (Et2O); dried (vac.); elem. anal.;
DOI:10.1016/S0020-1693(03)00304-9

Reference yield: 84.0%

: bis[dimethyl(μ-dimethylsulfide)platinum(II)]

: 361348-23-4
4-[(2-pyridinylmethylene)amino]benzenesulfonic acid sodium salt

: 613230-36-7
sodium 2-((4-sulfonatophenylimino)methyl)pyridine platinum(II) dimethyl

Guidance literature:: In dimethyl sulfoxide; Schlenk flask; mixt. was stirred overnight at room temp.; toluene was added, suspn. was stirred overnight, filtered, washed with toluene and CH2Cl2; elem. anal.;
DOI:10.1016/S0022-328X(03)00540-0