Cyclohexanone, 3-(3-butenyl)-

Base Information

• Chemical Name: Cyclohexanone, 3-(3-butenyl)-
• CAS No.: 3636-03-1
• Molecular Formula: C10H16O
• Molecular Weight: 152.236
• Hs Code.: 2914299000
• Mol file: 3636-03-1.mol

Synonyms:3-(Buten-(3)-yl)-cyclohexanon;3-(3-butenyl)cyclohexan-1-one;3-(3'-butenyl)cyclohexanone;Cyclohexanone,3-(3-butenyl);3-(But-3-enyl)-cyclohexanone;1--cyclohexanon-(3);

Chemical Property of Cyclohexanone, 3-(3-butenyl)-

Chemical Property:

• PSA: 17.07000
• LogP: 2.71190

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanone, 3-(3-butenyl)-

There total 10 articles about Cyclohexanone, 3-(3-butenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

((3-(but-3-en-1-yl)cyclohex-1-en-1-yl)oxy)trimethylsilane (145102-57-4) → 3-(3-butenyl)cyclohexan-1-one (3636-03-1) + 3-(3-butenyl)cyclohex-2-en-1-one (22627-45-8) + (3aS,7aS)-3-Methyl-1,3a,5,6,7,7a-hexahydro-inden-4-one

Guidance literature:

With oxygen; palladium diacetate; In dimethyl sulfoxide; at 45 ℃; under 760.051 Torr;

DOI:10.1021/ol020187u

Reference yield: 38.0%

1-methyl-3-(3-butenyl)cyclohexyl hydroperoxide (109323-25-3) → 3-(3-butenyl)cyclohexan-1-one (3636-03-1) + 3-But-3-enyl-1-methyl-cyclohexanol (109323-34-4) + 5-(3-methylcyclopentyl)-pentan-2-one (109323-28-6) + methyl (2-methyl-5-n-propyl)-cyclopentyl ketone (109323-31-1)

Guidance literature:

With iron(II) sulfate; In acetic acid; for 3h;

DOI:10.1016/S0040-4039(00)85378-2

Reference yield: 32.0%

3-But-3-enyl-1-phenyl-cyclohexyl-hydroperoxide (109323-27-5) → 3-(3-butenyl)cyclohexan-1-one (3636-03-1) + 4-(3-Methyl-cyclopentyl)-1-phenyl-butan-1-one (109323-30-0) + (2-Methyl-5-propyl-cyclopentyl)-phenyl-methanone (109323-33-3) + 3-But-3-enyl-1-phenyl-cyclohexanol (109323-36-6)

Guidance literature:

With iron(II) sulfate; In acetic acid; for 3h;

DOI:10.1016/S0040-4039(00)85378-2

upstream raw materials:

((3-(but-3-en-1-yl)cyclohex-1-en-1-yl)oxy)trimethylsilane

1-methyl-3-(3-butenyl)cyclohexyl hydroperoxide

3-But-3-enyl-1-ethyl-cyclohexyl-hydroperoxide

3-But-3-enyl-1-phenyl-cyclohexyl-hydroperoxide

Downstream raw materials:

1-(4-Brom-butyl)-cyclohexanon-⁽³⁾

3-(2-[1,2,4]Trioxolan-3-yl-ethyl)-cyclohexanone

3-(3-Oxo-butyl)-cyclohexanone

2-(3-Oxo-cyclohexylmethyl)-propenal

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