1-(Diphenylphosphoryloxymethyl)-4-methylbenzene

Base Information

Chemical Name:1-(Diphenylphosphoryloxymethyl)-4-methylbenzene
CAS No.:87671-55-4
Molecular Formula:C20H19 O2 P
Molecular Weight:322.343
Hs Code.:
NSC Number:171145
DSSTox Substance ID:DTXSID00305567
Nikkaji Number:J3.452.576E
Wikidata:Q82052230

Synonyms:87671-55-4;1-(diphenylphosphoryloxymethyl)-4-methylbenzene;NSC171145;DTXSID00305567;NSC-171145

Suppliers and Price of 1-(Diphenylphosphoryloxymethyl)-4-methylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-(Diphenylphosphoryloxymethyl)-4-methylbenzene

Chemical Property:

Vapor Pressure:3.38E-08mmHg at 25°C
Boiling Point:459.7°Cat760mmHg
Flash Point:245.1°C
Density:1.17g/cm³
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:322.11226684
Heavy Atom Count:23
Complexity:366

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)COP(=O)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of 1-(Diphenylphosphoryloxymethyl)-4-methylbenzene

There total 8 articles about 1-(Diphenylphosphoryloxymethyl)-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1707-03-5
diphenyl-phosphinic acid

: 104-81-4
4-Methylbenzyl bromide

: 87671-55-4
4-methylbenzyl phenyl(phenyl)phosphinate

Guidance literature:: With caesium carbonate; In acetonitrile; at 100 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2014.10.013

Reference yield: 92.0%

: 106-42-3
para-xylene

: 1707-03-5
diphenyl-phosphinic acid

: 87671-55-4
4-methylbenzyl phenyl(phenyl)phosphinate

Guidance literature:: With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; In dichloromethane; at 80 ℃; for 12h;
DOI:10.1021/acs.joc.7b02422

Reference yield: 90.0%

: 106-42-3
para-xylene

: 4559-70-0
Diphenylphosphine oxide

: 87671-55-4
4-methylbenzyl phenyl(phenyl)phosphinate

Guidance literature:: With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; at 90 ℃; for 12h; Schlenk technique;
DOI:10.1002/adsc.201400436