9,9-Bis(2-ethylhexyl)fluorene

Base Information

• Chemical Name: 9,9-Bis(2-ethylhexyl)fluorene
• CAS No.: 367524-07-0
• Molecular Formula: C29H42
• Molecular Weight: 390.652
• DSSTox Substance ID: DTXSID60407955
• Nikkaji Number: J1.130.506G
• Mol file: 367524-07-0.mol

Synonyms:9,9-bis(2-ethylhexyl)fluorene;367524-07-0;DTXSID60407955;MFCD03703236;9,9-BIS(2-ETHYLHEXYL)-9H-FLUORENE

Chemical Property of 9,9-Bis(2-ethylhexyl)fluorene

Chemical Property:

• XLogP3: 11.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 12
• Exact Mass: 390.328651340
• Heavy Atom Count: 29
• Complexity: 409

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCC(CC)CC1(C2=CC=CC=C2C3=CC=CC=C31)CC(CC)CCCC

Technology Process of 9,9-Bis(2-ethylhexyl)fluorene

There total 1 articles about 9,9-Bis(2-ethylhexyl)fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2,7-diiodo-9,9'-bis(2-ethylhexyl)fluorene (278176-08-2) + phenylboronic acid (98-80-6) → 9,9-bis-(2-ethyl-hexyl)-2-iodo-9H-fluorene + 2,7-bisphenyl-9,9'-bis(2-ethylhexyl)fluorene + 9,9-bis-(2-ethylhexyl)-9H-fluorene (367524-07-0)

Guidance literature:

With potassium phosphate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; tri-tert-butyl phosphine; In tetrahydrofuran; at 80 ℃; for 120h;

DOI:10.1021/ol061476b

upstream raw materials:

2,7-diiodo-9,9'-bis(2-ethylhexyl)fluorene

phenylboronic acid