Technology Process of 2-Butenoic acid, 2-Methyl-, phenylMethyl ester, (2Z)-
There total 4 articles about 2-Butenoic acid, 2-Methyl-, phenylMethyl ester, (2Z)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
caesium carbonate;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 6h;
Inert atmosphere;
DOI:10.1002/ejoc.201801193
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium hydroxide monohydrate / water; methanol / 4 h / Reflux
2: caesium carbonate / N,N-dimethyl-formamide / 6 h / 0 - 20 °C / Inert atmosphere
With
lithium hydroxide monohydrate; caesium carbonate;
In
methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201801193
- Guidance literature:
-
With
methanol; potassium carbonate;
anschliessend Erwaermen mit Benzyljodid;