Technology Process of Diazene, bis(4-propylphenyl)-, 1-oxide
There total 5 articles about Diazene, bis(4-propylphenyl)-, 1-oxide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide; acetic anhydride;
at 50 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 70.3 percent / NH4Cl, Zn / ethanol; H2O / 0.5 h / 40 - 45 °C
2: 94.4 percent / FeCl3 / ethanol; H2O / 10 °C
3: acetic acid; ethanol / 26 h / Ambient temperature
4: (Ac)2O, 30percent aq. H2O2 / 5 h / 50 °C
With
dihydrogen peroxide; acetic anhydride; iron(III) chloride; ammonium chloride; zinc;
In
ethanol; water; acetic acid;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetic acid; ethanol / 26 h / Ambient temperature
2: (Ac)2O, 30percent aq. H2O2 / 5 h / 50 °C
With
dihydrogen peroxide; acetic anhydride;
In
ethanol; acetic acid;