o-Nitrobenzylidene-p-chlorophenylacetonitrile

Base Information

• Chemical Name: o-Nitrobenzylidene-p-chlorophenylacetonitrile
• CAS No.: 104089-71-6
• Molecular Formula: C15H9 Cl N2 O2
• Molecular Weight: 284.702
• Mol file: 104089-71-6.mol

Synonyms:o-Nitrobenzylidene-p-chlorophenylacetonitrile;104089-71-6

Chemical Property of o-Nitrobenzylidene-p-chlorophenylacetonitrile

Chemical Property:

• Vapor Pressure: 3.75E-08mmHg at 25°C
• Boiling Point: 446.1°C at 760 mmHg
• Flash Point: 223.6°C
• Density: 1.357g/cm³
• XLogP3: 4.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 284.0352552
• Heavy Atom Count: 20
• Complexity: 427

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C=C(C#N)C2=CC=C(C=C2)Cl)[N+](=O)[O-]
• Isomeric SMILES: C1=CC=C(C(=C1)/C=C(\C#N)/C2=CC=C(C=C2)Cl)[N+](=O)[O-]

Technology Process of o-Nitrobenzylidene-p-chlorophenylacetonitrile

There total 3 articles about o-Nitrobenzylidene-p-chlorophenylacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Chloro-4-(chloromethyl)benzene (104-83-6) → 2-(4-chloro-phenyl)-3-(2-nitro-phenyl)-acrylonitrile (104089-71-6)

Guidance literature:

Multi-step reaction with 2 steps

1: alcohol; water

2: alcohol; alkali

With ethanol; water;

Reference yield:

toluene (108-88-3,15644-74-3,16713-13-6) → 2-(4-chloro-phenyl)-3-(2-nitro-phenyl)-acrylonitrile (104089-71-6)

Guidance literature:

Multi-step reaction with 3 steps

1: durch Chlorieren

2: alcohol; water

3: alcohol; alkali

With ethanol; water;

Reference yield:

2-nitro-benzaldehyde (552-89-6) + p-chlorobenzyl cyanide (140-53-4) → 2-(4-chloro-phenyl)-3-(2-nitro-phenyl)-acrylonitrile (104089-71-6)

Guidance literature:

With ethanol;

upstream raw materials:

2-nitro-benzaldehyde

p-chlorobenzyl cyanide

1-Chloro-4-(chloromethyl)benzene

toluene