O-[(3-Pyridyl)methyl]hydroxylamine

Base Information

Chemical Name:O-[(3-Pyridyl)methyl]hydroxylamine
CAS No.:37832-20-5
Molecular Formula:C₆H₈N₂O
Molecular Weight:124.142
Hs Code.:
European Community (EC) Number:833-486-5
DSSTox Substance ID:DTXSID40480746

Synonyms:O-[(3-Pyridyl)methyl]hydroxylamine;37832-20-5;O-(pyridin-3-ylmethyl)hydroxylamine;O-[(pyridin-3-yl)methyl]hydroxylamine;MFCD13175304;3-[(aminooxy)methyl]pyridine;SCHEMBL1520938;DTXSID40480746;Pyridine, 3-[(aminooxy)methyl]-;AC6038;AKOS017405216;SB75688;AS-60522;SY029692;CS-0156816;EN300-114693

Suppliers and Price of O-[(3-Pyridyl)methyl]hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of O-[(3-Pyridyl)methyl]hydroxylamine

Chemical Property:

XLogP3:-0.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:124.063662883
Heavy Atom Count:9
Complexity:77.5

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CN=C1)CON

Technology Process of O-[(3-Pyridyl)methyl]hydroxylamine

There total 3 articles about O-[(3-Pyridyl)methyl]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.2%

: 37832-20-5
O-(pyridin-3-ylmethyl)hydroxylamine

Guidance literature:

Reference yield:

: 30777-95-8
N-pyridin-3-ylmethoxy-phthalimide

: 37832-20-5
O-(pyridin-3-ylmethyl)hydroxylamine

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Reflux;
DOI:10.1021/jf072733+

Reference yield:

: 100-55-0
3-hydroxymethylpyridin

: 37832-20-5
O-(pyridin-3-ylmethyl)hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2: hydrazine hydrate / ethanol / 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; ethanol;
DOI:10.1021/ja402810t