Benzenamine, 4-[3-(9-anthracenyl)propyl]-N,N-dimethyl-

Base Information

• Chemical Name: Benzenamine, 4-[3-(9-anthracenyl)propyl]-N,N-dimethyl-
• CAS No.: 38474-11-2
• Molecular Formula: C25H25N
• Molecular Weight: 339.48
• Mol file: 38474-11-2.mol

Synonyms:1-(9-anthryl)-3-(4-(dimethylamino)phenyl)propane;1-(9-Anthryl)-3-(4-N,N-dimethylaniline)propane;Benzenamine,4-[3-(9-anthracenyl)propyl]-N,N-dimethyl;4-[3-(9-anthryl)propyl]-N,N-dimethylaniline;1-(9-anthryl)-3-(p-(N,N-dimethylamino)phenyl)propane;1-(9-anthryl)-3-(4-dimethylaniline)propane;1-(9-Anthryl)-3-(N,N-dimethylaniline)propane;

Chemical Property of Benzenamine, 4-[3-(9-anthracenyl)propyl]-N,N-dimethyl-

Chemical Property:

• PSA: 3.24000
• LogP: 6.23430

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenamine, 4-[3-(9-anthracenyl)propyl]-N,N-dimethyl-

There total 6 articles about Benzenamine, 4-[3-(9-anthracenyl)propyl]-N,N-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

1-(9-anthroyl)-2-(4-N,N-dimethylaniline) ethane (80525-77-5) → 4-[3-(9-anthryl)propyl]-N,N-dimethylaniline (38474-11-2)

Guidance literature:

With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; for 2h; Heating;

DOI:10.1246/bcsj.54.3304

Reference yield:

9-acetylanthracene (784-04-3) → 4-[3-(9-anthryl)propyl]-N,N-dimethylaniline (38474-11-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 95 percent / aq. 3M NaOH / aq. ethanol / 48 h

2: 90 percent / H₂ / 5percent Pd/C / acetone / 12 h / 2280 Torr

3: LiBEt₃H / tetrahydrofuran / a) RT, 30 min, b) reflux, 2 h

With sodium hydroxide; hydrogen; lithium triethylborohydride; palladium on activated charcoal; In tetrahydrofuran; ethanol; acetone;

DOI:10.1063/1.447925

Reference yield:

1-(9-anthroyl)-2-(4-N,N-dimethylaniline) ethylene (67805-12-3) → 4-[3-(9-anthryl)propyl]-N,N-dimethylaniline (38474-11-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / H₂ / 5percent Pd/C / acetone / 12 h / 2280 Torr

2: LiBEt₃H / tetrahydrofuran / a) RT, 30 min, b) reflux, 2 h

With hydrogen; lithium triethylborohydride; palladium on activated charcoal; In tetrahydrofuran; acetone;

DOI:10.1063/1.447925

upstream raw materials:

1-(9-anthroyl)-2-(4-N,N-dimethylaniline) ethane

9-acetylanthracene

1-(9-anthroyl)-2-(4-N,N-dimethylaniline) ethylene

4-dimethylamino-benzaldehyde