Silane, (3-chloropropyl)dimethyl[3-(1-phenylethenyl)phenyl]-

Base Information

• Chemical Name: Silane, (3-chloropropyl)dimethyl[3-(1-phenylethenyl)phenyl]-
• CAS No.: 384793-12-8
• Molecular Formula: C19H23ClSi
• Molecular Weight: 314.93
• DSSTox Substance ID: DTXSID30455963
• Nikkaji Number: J1.125.044K
• Wikidata: Q82278140
• Mol file: 384793-12-8.mol

Synonyms:384793-12-8;Silane, (3-chloropropyl)dimethyl[3-(1-phenylethenyl)phenyl]-;DTXSID30455963;alpha-(3-(Dimethyl(3-chloropropyl)silyl)phenyl)styrene

Chemical Property of Silane, (3-chloropropyl)dimethyl[3-(1-phenylethenyl)phenyl]-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 6
• Exact Mass: 314.1257550
• Heavy Atom Count: 21
• Complexity: 331

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C[Si](C)(CCCCl)C1=CC=CC(=C1)C(=C)C2=CC=CC=C2

Technology Process of Silane, (3-chloropropyl)dimethyl[3-(1-phenylethenyl)phenyl]-

There total 4 articles about Silane, (3-chloropropyl)dimethyl[3-(1-phenylethenyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-(3-bromophenyl)-1-phenylethylene (29265-79-0) + (3-chloropropyl)dimethylchlorosilane (10605-40-0) → 1-[3-((3-chloropropyl)dimethylsilyl)phenyl]-1-phenylethylene (384793-12-8)

Guidance literature:

1-(3-bromophenyl)-1-phenylethylene; With magnesium; In tetrahydrofuran; at 65 ℃; for 2h;

(3-chloropropyl)dimethylchlorosilane; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1021/ma021357l

Reference yield:

1-(3-bromo-phenyl)-1-phenyl-ethanol (90862-33-2) → 1-[3-((3-chloropropyl)dimethylsilyl)phenyl]-1-phenylethylene (384793-12-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran / 2 h / 65 °C

1.2: 87 percent / tetrahydrofuran / 12 h / 20 °C

With magnesium; In tetrahydrofuran;

DOI:10.1021/ma021357l

Reference yield:

phenylmagnesium bromide → 1-[3-((3-chloropropyl)dimethylsilyl)phenyl]-1-phenylethylene (384793-12-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: Mg / tetrahydrofuran / 2 h / 65 °C

1.2: 87 percent / tetrahydrofuran / 12 h / 20 °C

With magnesium; In tetrahydrofuran;

DOI:10.1021/ma021357l

upstream raw materials:

1-(3-bromophenyl)-1-phenylethylene

(3-chloropropyl)dimethylchlorosilane

1-(3-bromo-phenyl)-1-phenyl-ethanol

1-(3-Bromophenyl)ethanone

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