Benzenamine, 4-[(4-chlorophenyl)thio]-3,5-dimethyl-

Base Information

Chemical Name:Benzenamine, 4-[(4-chlorophenyl)thio]-3,5-dimethyl-
CAS No.:38560-98-4
Molecular Formula:C₁₄H₁₄ClNS
Molecular Weight:263.791
Hs Code.:
Mol file:38560-98-4.mol

Synonyms:

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Chemical Property of Benzenamine, 4-[(4-chlorophenyl)thio]-3,5-dimethyl-

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Technology Process of Benzenamine, 4-[(4-chlorophenyl)thio]-3,5-dimethyl-

There total 1 articles about Benzenamine, 4-[(4-chlorophenyl)thio]-3,5-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38560-98-4
4-Amino-4'-chlor-2,6-dimethyldiphenylsulfid

Guidance literature:: entspr. Acetamid, KOH;

Reference yield:

: 38560-98-4
4-Amino-4'-chlor-2,6-dimethyldiphenylsulfid

: 38560-69-9
2-[4-(4-chloro-benzenesulfinyl)-3,5-dimethyl-phenyl]-2H-[1,2,4]triazine-3,5-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) sodium nitrite, glacial acetic acid, concd. HCl, 2.) aq. acetic acid / 1.) 10 deg C, 15 min, 2.) RT, 1 h

2: sodium acetate, aq. H₂SO₄ / 6 h / Heating

3: aq. HCl / 1 h / Ambient temperature; pH 2.0

4: thioglycolic acid / 3 h / 140 °C

5: m-chloroperbenzoic acid / ethyl acetate

With hydrogenchloride; sulfuric acid; sodium acetate; acetic acid; mercaptoacetic acid; 3-chloro-benzenecarboperoxoic acid; sodium nitrite; In ethyl acetate;
DOI:10.1021/jm00143a015

Reference yield:

: 38560-98-4
4-Amino-4'-chlor-2,6-dimethyldiphenylsulfid

: 38560-80-4
2-[4-(4-chloro-benzenesulfonyl)-3,5-dimethyl-phenyl]-2H-[1,2,4]triazine-3,5-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) sodium nitrite, glacial acetic acid, concd. HCl, 2.) aq. acetic acid / 1.) 10 deg C, 15 min, 2.) RT, 1 h

2: sodium acetate, aq. H₂SO₄ / 6 h / Heating

3: aq. HCl / 1 h / Ambient temperature; pH 2.0

4: thioglycolic acid / 3 h / 140 °C

5: 92 percent / m-chloroperbenzoic acid / ethyl acetate / 1 h / Heating

With hydrogenchloride; sulfuric acid; sodium acetate; acetic acid; mercaptoacetic acid; 3-chloro-benzenecarboperoxoic acid; sodium nitrite; In ethyl acetate;
DOI:10.1021/jm00143a015