3-(2-(triMethylsilyl)ethynyl)phenol

Base Information

• Chemical Name: 3-(2-(triMethylsilyl)ethynyl)phenol
• CAS No.: 388061-72-1
• Molecular Formula: C11H14OSi
• Molecular Weight: 190.317
• Mol file: 388061-72-1.mol

Synonyms:3-TMSE-phenol;QC-1073;3-(2-(trimethylsilyl)ethynyl)phenol;3-[(trimethylsilyl)ethynyl]phenol;

Chemical Property of 3-(2-(triMethylsilyl)ethynyl)phenol

Chemical Property:

• Boiling Point: 260.6±32.0 °C(Predicted)
• PKA: 9.67±0.10(Predicted)
• PSA: 20.23000
• Density: 1.01±0.1 g/cm3(Predicted)
• LogP: 2.62110
• Storage Temp.: 2-8°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

3-((Trimethylsilyl)ethynyl)phenol 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 3-(2-(triMethylsilyl)ethynyl)phenol

There total 3 articles about 3-(2-(triMethylsilyl)ethynyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-Iodophenol (626-02-8) + trimethylsilylacetylene (1066-54-2) → 3-[2-(trimethylsilylethynyl)]phenol (388061-72-1)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 20 ℃; for 24h; Cooling with ice;

DOI:10.1016/j.cclet.2015.07.020

Reference yield:

3-Bromophenol (591-20-8) + trimethylsilylacetylene (1066-54-2) → 3-[2-(trimethylsilylethynyl)]phenol (388061-72-1)

Guidance literature:

With copper(l) iodide; bis(triphenylphosphine)palladium(II) dichloride; triethylamine; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ol503025n

Reference yield:

→ 3-[2-(trimethylsilylethynyl)]phenol (388061-72-1)

Guidance literature:

With triethylamine; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 0.333333h; Inert atmosphere;

With copper(l) iodide; In tetrahydrofuran; Inert atmosphere; Schlenk technique;

upstream raw materials:

3-Iodophenol

trimethylsilylacetylene

3-Bromophenol

Downstream raw materials:

1,4-bis(3-hydroxyphenyl)-1H-1,2,3-triazole

3,3'-(thiophene-2,5-diyl)diphenol

3-(4-(3-hydroxyphenyl)buta-1,3-diynyl)phenol

1,4-bis(3-glycidyloxyphenyl)-1H-1,2,3-triazole

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