5-METHYL-2-VINYLPYRIDINE

Base Information

• Chemical Name: 5-METHYL-2-VINYLPYRIDINE
• CAS No.: 3883-39-4
• Molecular Formula: C8H9N
• Molecular Weight: 119.166
• Hs Code.: 2933399090
• Mol file: 3883-39-4.mol

Synonyms:5-methyl-2-vinylfuran;Furan,2-ethenyl-5-methyl;3-methyl-6-vinylpyridinium;5-methyl-2-vinyl-pyridine;2-vinyl-5-methylfuran;Furan,2-methyl-5-vinyl;2-Methyl-5-vinylfuran;

Chemical Property of 5-METHYL-2-VINYLPYRIDINE

Chemical Property:

• Boiling Point: 100-102.5 °C(Press: 46 Torr)
• PKA: 5.09±0.10(Predicted)
• PSA: 12.89000
• Density: 0.954±0.06 g/cm3(Predicted)
• LogP: 2.03300

Purity/Quality:

97% ^*data from raw suppliers

5-Methyl-2-vinylpyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-METHYL-2-VINYLPYRIDINE

There total 5 articles about 5-METHYL-2-VINYLPYRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

→ 3-methyl-6-vinylpyridinium (3883-39-4)

Guidance literature:

Reference yield: 89.0%

2-Bromo-5-methylpyridine (3510-66-5) + potassium vinyltrifluoroborate → 3-methyl-6-vinylpyridinium (3883-39-4)

Guidance literature:

With potassium phosphate monohydrate; palladium diacetate; N₂Phos; In water; toluene; at 45 ℃; for 16h;

DOI:10.1039/d0sc00968g

Reference yield: 75.6%

2-Bromo-5-methylpyridine (3510-66-5) + trivinylboroxin (92988-08-4) → 3-methyl-6-vinylpyridinium (3883-39-4)

Guidance literature:

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; at 100 ℃; Inert atmosphere;

upstream raw materials:

2-Bromo-5-methylpyridine

tri-n-butyl(vinyl)tin

trivinylboroxin

5-methylpicolinaldehyde

Downstream raw materials:

4-[2-(5-Methyl-pyridin-2-yl)-ethylsulfanyl]-phenylamine

2-(1-benzyl-pyrrolidin-3-yl)-5-methyl-pyridine

N-(2-(5-methylpyridin-2-yl)ethyl)benzenesulfonamide

3-(5-Methyl-pyridin-2-yl)-1-phenyl-propan-1-one

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