Hexanoic acid, 2,3-dioxo-, ethyl ester

Base Information

• Chemical Name: Hexanoic acid, 2,3-dioxo-, ethyl ester
• CAS No.: 3885-41-4
• Molecular Formula: C8H12O4
• Molecular Weight: 172.181
• Mol file: 3885-41-4.mol

Synonyms:Butyrylglyoxylsaeureethylester;2,3-dioxo-hexanoic acid ethyl ester;α,β-Dioxo-n-capronsaeure-aethylester;2,3-Dioxo-hexansaeure-aethylester;Butyrylglyoxylsaeure-aethylester;

Chemical Property of Hexanoic acid, 2,3-dioxo-, ethyl ester

Chemical Property:

• Melting Point: 55-57 °C
• Boiling Point: 83-86 °C(Press: 10 Torr)
• PSA: 60.44000
• Density: 1.104 g/cm3(Temp: 0 °C)
• LogP: 0.48780

Purity/Quality:

95% ^*data from raw suppliers

Ethyl2,3-dioxohexanoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hexanoic acid, 2,3-dioxo-, ethyl ester

There total 8 articles about Hexanoic acid, 2,3-dioxo-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

ethyl 2-(benzyloxyimino)-3-oxohexanoate → ethyl 2,3-dioxohexanoate (3885-41-4)

Guidance literature:

With acetic acid; zinc; at 20 ℃; for 1h;

DOI:10.1246/bcsj.77.1407

Reference yield:

ethyl 2-acetoxy-2-chloro-3-oxohexanoate (865445-61-0) → ethyl 2,3-dioxohexanoate (3885-41-4)

Guidance literature:

With hydrogenchloride; In ethanol; at 20 ℃; for 16h;

DOI:10.1016/j.tet.2008.11.090

Reference yield:

ethyl 2-picolinoyl-3-oxo-3-hexanoate (953420-14-9) → ethyl 2,3-dioxohexanoate (3885-41-4)

Guidance literature:

With ethanol; copper diacetate; In dichloromethane; at 20 ℃;

DOI:10.1016/j.tetlet.2007.07.153

upstream raw materials:

ethyl butyroyl acetate

Butyrylglyoxylsaeure-aethylester-triphenylphosphazin-⁽²⁾

ethyl 3-oxo-2-(triphenylphosphoranylidene)-4-hexenoate

acetic anhydride

Downstream raw materials:

2-phenyl-5-propyl-2H-pyrazole-3,4-dione-4-oxime

ethyl 3-phenyl-5-propyl-1,2,4-triazine-6-carboxylate

ethyl 2-(4-methoxyphenyl)-4-propylimidazole-5-carboxylate

ethyl 2-(4-chlorophenyl)-4-propylimidazole-5-carboxylate

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