4H-Cyclohepta[b]thiophene-3-carboxylic acid, 2-[[[(4-chlorophenyl)amino]thioxomethyl]amino]-5,6,7,8-tetrahydro-, ethyl ester

Base Information

Chemical Name:4H-Cyclohepta[b]thiophene-3-carboxylic acid, 2-[[[(4-chlorophenyl)amino]thioxomethyl]amino]-5,6,7,8-tetrahydro-, ethyl ester
CAS No.:389088-14-6
Molecular Formula:C₁₉H₂₁ClN₂O₂S₂
Molecular Weight:408.973
Hs Code.:
Mol file:389088-14-6.mol

Synonyms:

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Chemical Property of 4H-Cyclohepta[b]thiophene-3-carboxylic acid, 2-[[[(4-chlorophenyl)amino]thioxomethyl]amino]-5,6,7,8-tetrahydro-, ethyl ester

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Technology Process of 4H-Cyclohepta[b]thiophene-3-carboxylic acid, 2-[[[(4-chlorophenyl)amino]thioxomethyl]amino]-5,6,7,8-tetrahydro-, ethyl ester

There total 1 articles about 4H-Cyclohepta[b]thiophene-3-carboxylic acid, 2-[[[(4-chlorophenyl)amino]thioxomethyl]amino]-5,6,7,8-tetrahydro-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40106-13-6
2-amino-5,6,7,8-tetrahydro-4H-cyclohepta[b]thiophene-3-carboxylic acid ethyl ester

: 2131-55-7
4-Chlorophenyl isothiocyanate

: 389088-14-6
2-[3-(4-chloro-phenyl)-thioureido]-5,6,7,8-tetrahydro-4H-cyclohepta[b]thiophene-3-carboxylic acid ethyl ester

Guidance literature:: In ethanol; Heating;
DOI:10.3390/11070498

Reference yield:

: 389088-14-6
2-[3-(4-chloro-phenyl)-thioureido]-5,6,7,8-tetrahydro-4H-cyclohepta[b]thiophene-3-carboxylic acid ethyl ester

: 3-(4-chlorophenyl)-2-thioxo-1,2,3,5,6,7,8,9-octahydrocyclohepta[4,5]thieno[2,3-d]pyrimidin-4-one

Guidance literature:: 2-[3-(4-chloro-phenyl)-thioureido]-5,6,7,8-tetrahydro-4H-cyclohepta[b]thiophene-3-carboxylic acid ethyl ester; With potassium hydroxide; In ethanol; for 1h; Heating;

With hydrogenchloride; at 20 ℃; for 0.5h;
DOI:10.3390/11070498

Reference yield:

: 389088-14-6
2-[3-(4-chloro-phenyl)-thioureido]-5,6,7,8-tetrahydro-4H-cyclohepta[b]thiophene-3-carboxylic acid ethyl ester

: 2-benzylthio-3-(4-chlorophenyl)-3,5,6,7,8,9-hexahydrocyclohepta[4,5]thieno[2,3-d]pyrimidin-4-one

Guidance literature:: 2-[3-(4-chloro-phenyl)-thioureido]-5,6,7,8-tetrahydro-4H-cyclohepta[b]thiophene-3-carboxylic acid ethyl ester; With potassium hydroxide; In ethanol; Heating;

C₆H₅CH₂-halide; In ethanol; for 8h; Heating;
DOI:10.3390/11070498