1(2H)-Pyridinecarboxylic acid, 3-(acetyloxy)-3,4-dihydro-4-oxo-2-[(phenylmethoxy)methyl]-, phenylmethyl ester, (2R,3R)-

Base Information

Chemical Name:1(2H)-Pyridinecarboxylic acid, 3-(acetyloxy)-3,4-dihydro-4-oxo-2-[(phenylmethoxy)methyl]-, phenylmethyl ester, (2R,3R)-
CAS No.:389092-27-7
Molecular Formula:C23H23NO6
Molecular Weight:409.439
Hs Code.:
Mol file:389092-27-7.mol

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Chemical Property of 1(2H)-Pyridinecarboxylic acid, 3-(acetyloxy)-3,4-dihydro-4-oxo-2-[(phenylmethoxy)methyl]-, phenylmethyl ester, (2R,3R)-

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Technology Process of 1(2H)-Pyridinecarboxylic acid, 3-(acetyloxy)-3,4-dihydro-4-oxo-2-[(phenylmethoxy)methyl]-, phenylmethyl ester, (2R,3R)-

There total 6 articles about 1(2H)-Pyridinecarboxylic acid, 3-(acetyloxy)-3,4-dihydro-4-oxo-2-[(phenylmethoxy)methyl]-, phenylmethyl ester, (2R,3R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 546-67-8
lead(IV) tetraacetate

: 389092-25-5
2-benzyloxymethyl-4-oxo-3,4-dihydro-2H-pyridine-1-carboxylic acid benzyl ester

: 389092-27-7
(2R,3R)-3-Acetoxy-2-benzyloxymethyl-4-oxo-3,4-dihydro-2H-pyridine-1-carboxylic acid benzyl ester

Guidance literature:: In toluene; for 22h; Heating;
DOI:10.1016/S0040-4039(01)01432-0

Reference yield:

: 126378-42-5
4-methoxy-3-(trisopropylsilyl)pyridine

: 389092-27-7
(2R,3R)-3-Acetoxy-2-benzyloxymethyl-4-oxo-3,4-dihydro-2H-pyridine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.2: H₃O⁽¹⁺⁾

2.1: NaOMe

2.2: 74 percent / H₃O⁽¹⁺⁾

3.1: 99 percent / n-BuLi

4.1: 78 percent / toluene / 22 h / Heating

With n-butyllithium; sodium methylate; In toluene;
DOI:10.1016/S0040-4039(01)01432-0

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 389092-27-7
(2R,3R)-3-Acetoxy-2-benzyloxymethyl-4-oxo-3,4-dihydro-2H-pyridine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / n-BuLi

2: 78 percent / toluene / 22 h / Heating

With n-butyllithium; In toluene;
DOI:10.1016/S0040-4039(01)01432-0