Pyrrolo[3,4-c]carbazole-5-carboxylic acid, 1,2,3,6-tetrahydro-2-methyl-6-[(4-methylphenyl)sulfonyl]-1-oxo-, methyl ester

Base Information

Chemical Name:Pyrrolo[3,4-c]carbazole-5-carboxylic acid, 1,2,3,6-tetrahydro-2-methyl-6-[(4-methylphenyl)sulfonyl]-1-oxo-, methyl ester
CAS No.:389118-14-3
Molecular Formula:C24H20N2O5S
Molecular Weight:448.499
Hs Code.:
Mol file:389118-14-3.mol

Synonyms:

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Chemical Property of Pyrrolo[3,4-c]carbazole-5-carboxylic acid, 1,2,3,6-tetrahydro-2-methyl-6-[(4-methylphenyl)sulfonyl]-1-oxo-, methyl ester

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Technology Process of Pyrrolo[3,4-c]carbazole-5-carboxylic acid, 1,2,3,6-tetrahydro-2-methyl-6-[(4-methylphenyl)sulfonyl]-1-oxo-, methyl ester

There total 2 articles about Pyrrolo[3,4-c]carbazole-5-carboxylic acid, 1,2,3,6-tetrahydro-2-methyl-6-[(4-methylphenyl)sulfonyl]-1-oxo-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 389118-13-2
4-(methyl-prop-2-ynyl-carbamoyl)-9-(toluene-4-sulfonyl)-9H-2,3,9-triaza-fluorene-1-carboxylic acid methyl ester

: 389118-14-3
2-methyl-1-oxo-6-(toluene-4-sulfonyl)-1,2,3,6-tetrahydro-pyrrolo[3,4-c]carbazole-5-carboxylic acid methyl ester

Guidance literature:: With 2,6-di-tert-butyl-4-methyl-phenol; In diethylene glycol dimethyl ether; Heating;
DOI:10.1016/S0040-4039(01)01678-1

Reference yield:

: 9-(toluene-4-sulfonyl)-9H-2,3,9-triaza-fluorene-1,4-dicarboxylic acid dimethyl ester

: 389118-14-3
2-methyl-1-oxo-6-(toluene-4-sulfonyl)-1,2,3,6-tetrahydro-pyrrolo[3,4-c]carbazole-5-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / AlMe₃

2: 90 percent / BHT / bis-(2-methoxy-ethyl) ether / Heating

With 2,6-di-tert-butyl-4-methyl-phenol; trimethylaluminum; In diethylene glycol dimethyl ether; 1: Weinreb amidation / 2: intramolecular Diels-Alder addition;
DOI:10.1016/S0040-4039(01)01678-1