Acetamide, N-[3-(5-cyclobutyl-1,3,4,5-tetrahydro-5-hydroxy-4-oxo-2H-2-benzazepin -2-yl)propyl]-2,2,2-trifluoro-N-(phenylmethyl)-

Base Information

Chemical Name:Acetamide, N-[3-(5-cyclobutyl-1,3,4,5-tetrahydro-5-hydroxy-4-oxo-2H-2-benzazepin -2-yl)propyl]-2,2,2-trifluoro-N-(phenylmethyl)-
CAS No.:391198-74-6
Molecular Formula:C26H29F3N2O3
Molecular Weight:474.523
Hs Code.:
Mol file:391198-74-6.mol

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Chemical Property of Acetamide, N-[3-(5-cyclobutyl-1,3,4,5-tetrahydro-5-hydroxy-4-oxo-2H-2-benzazepin -2-yl)propyl]-2,2,2-trifluoro-N-(phenylmethyl)-

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Technology Process of Acetamide, N-[3-(5-cyclobutyl-1,3,4,5-tetrahydro-5-hydroxy-4-oxo-2H-2-benzazepin -2-yl)propyl]-2,2,2-trifluoro-N-(phenylmethyl)-

There total 2 articles about Acetamide, N-[3-(5-cyclobutyl-1,3,4,5-tetrahydro-5-hydroxy-4-oxo-2H-2-benzazepin -2-yl)propyl]-2,2,2-trifluoro-N-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: N-Benzyl-N-[3-(5-cyclobutyl-4,5-dihydroxy-1,3,4,5-tetrahydrobenzo[c]azepin-2-yl)propyl]-2,2,2-trifluoroacetamide

: 391198-74-6
5-cyclobutyl-5-hydroxy-2-[3-(N-phenylmethyl-N-trifluoroacetyl)aminopropyl]-2,3,4,5-tetrahydro-[1H]-2-benzazepin-4-one

Guidance literature:: With (COCl)2; triethanolamine; In diethyl ether; water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; dimethyl sulfoxide;

Reference yield: 67.0%

: (4SR,5RS)-5-cyclobutyl-4,5-dihydroxy-2-[3-(N-phenylmethyl-N-trifluoroacetyl)aminopropyl]-2,3,4,5-tetrahydro-[1H]-2-benzazepine

: 391198-74-6
5-cyclobutyl-5-hydroxy-2-[3-(N-phenylmethyl-N-trifluoroacetyl)aminopropyl]-2,3,4,5-tetrahydro-[1H]-2-benzazepin-4-one

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1039/b801206g