Benzenebutanamine, 4-methoxy-, hydrochloride

Base Information

Chemical Name:Benzenebutanamine, 4-methoxy-, hydrochloride
CAS No.:391202-29-2
Molecular Formula:C11H17NO.ClH
Molecular Weight:215.723
Hs Code.:
Mol file:391202-29-2.mol

Synonyms:1-(4-aminobutyl)-4-methoxybenzene hydrochloride;

Suppliers and Price of Benzenebutanamine, 4-methoxy-, hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenebutanamine, 4-methoxy-, hydrochloride

Chemical Property:

PSA：35.25000
LogP:3.47890

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzenebutanamine, 4-methoxy-, hydrochloride

There total 5 articles about Benzenebutanamine, 4-methoxy-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2N-potassium hydroxide: 2N-potassium hydroxide

: 391202-28-1
4-amino-4'-methoxybutyrophenone trifluoromethanesulfonate

: 108-20-3
di-isopropyl ether

: 67-63-0,8013-70-5
isopropyl alcohol

: 391202-29-2
4-(4-methoxyphenyl)butan-1-amine hydrochloride

Guidance literature:: With hydrogenchloride; palladium-carbon; In tetrahydrofuran; toluene;

Reference yield:

: 211692-42-1
2-[4-(4-methoxy-phenyl)-butyl]-isoindole-1,3-dione

: 391202-29-2
4-(4-methoxyphenyl)butan-1-amine hydrochloride

Guidance literature:: 2-[4-(4-methoxy-phenyl)-butyl]-isoindole-1,3-dione; With hydrazine hydrate; In ethanol; at 78 ℃; for 3h;

With hydrogenchloride; In water;
DOI:10.1021/acs.jmedchem.5b01188

Reference yield:

: 52244-70-9,239474-80-7
4-(4-methoxyphenyl)butan-1-ol

: 391202-29-2
4-(4-methoxyphenyl)butan-1-amine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine; diethylazodicarboxylate / toluene; tetrahydrofuran / 15 h / 0 - 20 °C / Inert atmosphere

2.1: hydrazine hydrate / ethanol / 3 h / 78 °C

2.2: Gabriel Amine Synthesis

With hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; toluene; 2.1: |Gabriel Amine Synthesis;
DOI:10.1021/acs.jmedchem.5b01188