2-Furanmethanol, 4-(benzoyloxy)tetrahydro-a-8-nonenyl-5-pentyl-, (2S,4S,5S)-

Base Information

Chemical Name:2-Furanmethanol, 4-(benzoyloxy)tetrahydro-a-8-nonenyl-5-pentyl-, (2S,4S,5S)-
CAS No.:391232-90-9
Molecular Formula:C₂₆H₄₀O₄
Molecular Weight:416.601
Hs Code.:

Synonyms:

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Chemical Property of 2-Furanmethanol, 4-(benzoyloxy)tetrahydro-a-8-nonenyl-5-pentyl-, (2S,4S,5S)-

Chemical Property:

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Technology Process of 2-Furanmethanol, 4-(benzoyloxy)tetrahydro-a-8-nonenyl-5-pentyl-, (2S,4S,5S)-

There total 6 articles about 2-Furanmethanol, 4-(benzoyloxy)tetrahydro-a-8-nonenyl-5-pentyl-, (2S,4S,5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 391232-77-2
methyl 3-O-benzoyl-5-O-benzyl-3-deoxy-α-D-threo-pentofuranoside

: 391232-90-9
(6S,7S,9S,10R/S)-6,9-epoxynonadec-18-ene-7-O-benzoyloxy-10-ol

Guidance literature:: Multi-step reaction with 6 steps

1.1: TMSOTf / acetonitrile / 4 h / -20 °C

2.1: N-methylmorpholine oxide; OsO₄ / acetone; H₂O / 20 °C

2.2: NaIO₄; SiO₂ / CH₂Cl₂; H₂O / 20 °C

3.1: NaNH₂ / tetrahydrofuran / 12 h / 20 °C

3.2: 441 mg / tetrahydrofuran / 1 h / -20 °C

4.1: 91 percent / H₂ / 10percent Pd/C / methanol / 6 h

5.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -78 °C

6.1: 214 mg / tetrahydrofuran; diethyl ether / 4 h / 20 °C

With osmium(VIII) oxide; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; hydrogen; sodium amide; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; 10percent Pd/C; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; acetonitrile; 5.1: Swern oxidation / 6.1: Grignard reaction;
DOI:10.1021/jo010830a

Reference yield:

: Benzoic acid (2S,3S,5S)-5-benzyloxymethyl-2-(2-oxo-ethyl)-tetrahydro-furan-3-yl ester

: 391232-90-9
(6S,7S,9S,10R/S)-6,9-epoxynonadec-18-ene-7-O-benzoyloxy-10-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaNH₂ / tetrahydrofuran / 12 h / 20 °C

1.2: 441 mg / tetrahydrofuran / 1 h / -20 °C

2.1: 91 percent / H₂ / 10percent Pd/C / methanol / 6 h

3.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -78 °C

4.1: 214 mg / tetrahydrofuran; diethyl ether / 4 h / 20 °C

With oxalyl dichloride; hydrogen; sodium amide; dimethyl sulfoxide; triethylamine; 10percent Pd/C; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 3.1: Swern oxidation / 4.1: Grignard reaction;
DOI:10.1021/jo010830a

Reference yield:

: 391232-78-3
2-allyl-5-benzyloxymethyl-3-phenylcarbonyloxy-(2S,3S,5S)-tetrahydrofuran

: 391232-90-9
(6S,7S,9S,10R/S)-6,9-epoxynonadec-18-ene-7-O-benzoyloxy-10-ol

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-methylmorpholine oxide; OsO₄ / acetone; H₂O / 20 °C

1.2: NaIO₄; SiO₂ / CH₂Cl₂; H₂O / 20 °C

2.1: NaNH₂ / tetrahydrofuran / 12 h / 20 °C

2.2: 441 mg / tetrahydrofuran / 1 h / -20 °C

3.1: 91 percent / H₂ / 10percent Pd/C / methanol / 6 h

4.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -78 °C

5.1: 214 mg / tetrahydrofuran; diethyl ether / 4 h / 20 °C

With osmium(VIII) oxide; oxalyl dichloride; hydrogen; sodium amide; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; 10percent Pd/C; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; 4.1: Swern oxidation / 5.1: Grignard reaction;
DOI:10.1021/jo010830a