[4-(4-Bromophenoxy)phenyl]phosphonic dichloride

Base Information

Chemical Name:[4-(4-Bromophenoxy)phenyl]phosphonic dichloride
CAS No.:391642-69-6
Molecular Formula:C12H8BrCl2O2P
Molecular Weight:365.978
Hs Code.:
DSSTox Substance ID:DTXSID30595313
Wikidata:Q82490306
Mol file:391642-69-6.mol

Synonyms:391642-69-6;[4-(4-Bromophenoxy)phenyl]phosphonic dichloride;SCHEMBL6821577;DTXSID30595313

Suppliers and Price of [4-(4-Bromophenoxy)phenyl]phosphonic dichloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [4-(4-Bromophenoxy)phenyl]phosphonic dichloride

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:363.88223
Heavy Atom Count:18
Complexity:307

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1OC2=CC=C(C=C2)Br)P(=O)(Cl)Cl

Technology Process of [4-(4-Bromophenoxy)phenyl]phosphonic dichloride

There total 2 articles about [4-(4-Bromophenoxy)phenyl]phosphonic dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₆BrO₄PSi₂

: 391642-69-6
4-(4-bromophenoxy)phenylphosphonic dichloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2003.09.015

Reference yield:

: diethyl 4-(4-bromophenoxy)phenylphosphonate

: 391642-69-6
4-(4-bromophenoxy)phenylphosphonic dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / acetonitrile / 0.75 h / 40 °C

2: oxalyl chloride; DMF / CH₂Cl₂ / 1 h / 20 °C

With oxalyl dichloride; N,N-dimethyl-formamide; sodium iodide; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2003.09.015