Imidazo[4,5-c]carbazole-4-carbothioic acid, 1,6-dihydro-1-[(phenylmethoxy)methyl]-6-(phenylsulfonyl)-, S-phenyl ester

Base Information

Chemical Name:Imidazo[4,5-c]carbazole-4-carbothioic acid, 1,6-dihydro-1-[(phenylmethoxy)methyl]-6-(phenylsulfonyl)-, S-phenyl ester
CAS No.:391913-54-5
Molecular Formula:C34H25N3O4S2
Molecular Weight:603.722
Hs Code.:
Mol file:391913-54-5.mol

Synonyms:

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Chemical Property of Imidazo[4,5-c]carbazole-4-carbothioic acid, 1,6-dihydro-1-[(phenylmethoxy)methyl]-6-(phenylsulfonyl)-, S-phenyl ester

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Technology Process of Imidazo[4,5-c]carbazole-4-carbothioic acid, 1,6-dihydro-1-[(phenylmethoxy)methyl]-6-(phenylsulfonyl)-, S-phenyl ester

There total 3 articles about Imidazo[4,5-c]carbazole-4-carbothioic acid, 1,6-dihydro-1-[(phenylmethoxy)methyl]-6-(phenylsulfonyl)-, S-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 108-98-5
thiophenol

: 391913-74-9
6-benzenesulfonyl-1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluorene-4-carboxylic acid

: 391913-54-5
6-benzenesulfonyl-1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluorene-4-carbothioic acid S-phenyl ester

Guidance literature:: With Carbonyldiimidazole; In N,N-dimethyl-formamide; at -10 ℃; for 2h;
DOI:10.1016/S0040-4039(01)01915-3

Reference yield:

: 391913-53-4
6-benzenesulfonyl-1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluorene-4-carboxylic acid ethyl ester

: 391913-54-5
6-benzenesulfonyl-1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluorene-4-carbothioic acid S-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / LiOH / tetrahydrofuran; H₂O; methanol / 5 h / 20 °C

2: 58 percent / carbonyl-diimidazole / dimethylformamide / 2 h / -10 °C

With lithium hydroxide; Carbonyldiimidazole; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)01915-3

Reference yield:

: 391913-72-7
6-benzenesulfonyl-1-benzyloxymethyl-2-phenylsulfanyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluorene-4-carboxylic acid ethyl ester

: 391913-54-5
6-benzenesulfonyl-1-benzyloxymethyl-1,6-dihydro-1,3,6-triaza-cyclopenta[c]fluorene-4-carbothioic acid S-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / Raney-Ni / ethanol; tetrahydrofuran / 2 h / Heating

2: 91 percent / LiOH / tetrahydrofuran; H₂O; methanol / 5 h / 20 °C

3: 58 percent / carbonyl-diimidazole / dimethylformamide / 2 h / -10 °C

With lithium hydroxide; Carbonyldiimidazole; nickel; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)01915-3