7-Octene-2,6-diol, 2,6-dimethyl-, (6R)-

Base Information

Chemical Name:7-Octene-2,6-diol, 2,6-dimethyl-, (6R)-
CAS No.:392298-14-5
Molecular Formula:C10H20O2
Molecular Weight:
Hs Code.:
Mol file:392298-14-5.mol

Synonyms:

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Chemical Property of 7-Octene-2,6-diol, 2,6-dimethyl-, (6R)-

Chemical Property:

Purity/Quality:

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Technology Process of 7-Octene-2,6-diol, 2,6-dimethyl-, (6R)-

There total 10 articles about 7-Octene-2,6-diol, 2,6-dimethyl-, (6R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₃NO₂

: 392298-14-5,57784-11-9
(R)-2,6-dimethyl-oct-7-ene-2,6-diol

Guidance literature:: With acetic acid; zinc; In tetrahydrofuran; water; at 50 ℃; for 5h; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.202001725

Reference yield:

: (E)-N,N-dibenzyl-5-(3,3-dimethyloxiran-2-yl)-3-methylpent-2-en-1-amine

: 392298-14-5,57784-11-9
(R)-2,6-dimethyl-oct-7-ene-2,6-diol

Guidance literature:: Multi-step reaction with 4 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h / -20 °C / Inert atmosphere

2: C₁₁₆H₁₀₀Fe₂N₈O₁₆Pd₄S₄ / dichloromethane / 120 h / 0 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 40 °C / Inert atmosphere

4: zinc; acetic acid / tetrahydrofuran; water / 5 h / 50 °C / Inert atmosphere

With lithium aluminium tetrahydride; C₁₁₆H₁₀₀Fe₂N₈O₁₆Pd₄S₄; acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/anie.202001725

Reference yield:

: (Z)-N,N-dibenzyl-5-(3,3-dimethyloxiran-2-yl)-3-methylpent-2-en-1-amine

: 392298-14-5,57784-11-9
(R)-2,6-dimethyl-oct-7-ene-2,6-diol

Guidance literature:: Multi-step reaction with 4 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h / -20 °C / Inert atmosphere

2: C₁₁₆H₁₀₀Fe₂N₈O₁₆Pd₄S₄ / dichloromethane / 120 h / 0 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 40 °C / Inert atmosphere

4: zinc; acetic acid / tetrahydrofuran; water / 5 h / 50 °C / Inert atmosphere

With lithium aluminium tetrahydride; C₁₁₆H₁₀₀Fe₂N₈O₁₆Pd₄S₄; acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/anie.202001725