4-Imidazolidinecarboxylic acid, 3-[(2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-methyl-1-oxobutyl]-2- oxo-1-(phenylmethyl)-, (4S)-

Base Information

Chemical Name:4-Imidazolidinecarboxylic acid, 3-[(2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-methyl-1-oxobutyl]-2- oxo-1-(phenylmethyl)-, (4S)-
CAS No.:393548-65-7
Molecular Formula:C₂₁H₂₉N₃O₆
Molecular Weight:419.478
Hs Code.:
Mol file:393548-65-7.mol

Synonyms:

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Chemical Property of 4-Imidazolidinecarboxylic acid, 3-[(2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-methyl-1-oxobutyl]-2- oxo-1-(phenylmethyl)-, (4S)-

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Technology Process of 4-Imidazolidinecarboxylic acid, 3-[(2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-methyl-1-oxobutyl]-2- oxo-1-(phenylmethyl)-, (4S)-

There total 1 articles about 4-Imidazolidinecarboxylic acid, 3-[(2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-methyl-1-oxobutyl]-2- oxo-1-(phenylmethyl)-, (4S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89371-88-0
benzyl (4S)-1-benzyl-3-benzyloxycarbonyl-2-oxo-imidazolidine-4-carboxylate

: 393548-65-7
(S)-1-Benzyl-3-((S)-2-tert-butoxycarbonylamino-3-methyl-butyryl)-2-oxo-imidazolidine-4-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: HBr; AcOH

2.1: KO-tBu / tetrahydrofuran / -40 °C

2.2: tetrahydrofuran / -40 °C

3.1: 100 percent / H₂ / Pd/C / ethanol

With potassium tert-butylate; hydrogen bromide; hydrogen; acetic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmcl.2004.09.058

Reference yield: 91.0%

: 3-amino-2-hydroxy-hexanoic acid allylamide hydrochloride

: 393548-65-7
(S)-1-Benzyl-3-((S)-2-tert-butoxycarbonylamino-3-methyl-butyryl)-2-oxo-imidazolidine-4-carboxylic acid

: 811803-64-2
((S)-1-{(S)-5-[1-(Allylcarbamoyl-hydroxy-methyl)-butylcarbamoyl]-3-benzyl-2-oxo-imidazolidine-1-carbonyl}-2-methyl-propyl)-carbamic acid tert-butyl ester

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
DOI:10.1016/j.bmcl.2004.09.058

Reference yield: 64.0%

: 393548-65-7
(S)-1-Benzyl-3-((S)-2-tert-butoxycarbonylamino-3-methyl-butyryl)-2-oxo-imidazolidine-4-carboxylic acid

: (3-amino-2-hydroxy-hexanoylamino)-acetic acid allyl ester; hydrochloride

: 393548-68-0
(3-{[(S)-1-Benzyl-3-((S)-2-tert-butoxycarbonylamino-3-methyl-butyryl)-2-oxo-imidazolidine-4-carbonyl]-amino}-2-hydroxy-hexanoylamino)-acetic acid allyl ester

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
DOI:10.1016/j.bmcl.2004.09.058