(3-Chloro-2-methylphenyl)hydrazine

Base Information

• Chemical Name: (3-Chloro-2-methylphenyl)hydrazine
• CAS No.: 39943-64-1
• Molecular Formula: C7H9ClN2
• Molecular Weight: 156.615
• DSSTox Substance ID: DTXSID90351538
• Nikkaji Number: J411.622D
• Wikidata: Q82128027
• Mol file: 39943-64-1.mol

Synonyms:(3-chloro-2-methylphenyl)hydrazine;39943-64-1;(3-CHLORO-2-METHYL-PHENYL)-HYDRAZINE;Hydrazine, (3-chloro-2-methylphenyl)-;3-chloro-2-methylphenylhydrazine;1-(3-chloro-2-methylphenyl)hydrazine;TimTec1_005812;SCHEMBL1143322;DTXSID90351538;3-chloro-2-methylphenyl hydrazine;OTKORKMZHLQZQS-UHFFFAOYSA-N;HMS1550I04;AM9801;STK501157;AKOS000112917;BS-3864;SB75886;NCGC00173486-01;BB 0219958

Chemical Property of (3-Chloro-2-methylphenyl)hydrazine

Chemical Property:

• Vapor Pressure: 0.0205mmHg at 25°C
• Boiling Point: 251.4oC at 760 mmHg
• PKA: 5.05±0.10(Predicted)
• Flash Point: 105.9oC
• PSA: 38.05000
• Density: 1.26g/cm3
• LogP: 2.70730
• Storage Temp.: 2-8°C
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 156.0454260
• Heavy Atom Count: 10
• Complexity: 108

Purity/Quality:

98%Min ^*data from raw suppliers

(3-chloro-2-methyl-phenyl)-hydrazine 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=CC=C1Cl)NN

Technology Process of (3-Chloro-2-methylphenyl)hydrazine

There total 2 articles about (3-Chloro-2-methylphenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

3-chloro-2-methylbenzenamine (87-60-5) → (3-chloro-2-methylphenyl)hydrazine (39943-64-1)

Guidance literature:

3-chloro-2-methylbenzenamine; With hydrogenchloride; trifluoroacetic acid; In water; at 20 ℃; for 0.166667h;

With sodium nitrite; In water; at 0 ℃; for 1h;

With hydrogenchloride; tin(ll) chloride; In water; at 20 ℃;

Reference yield:

→ (3-chloro-2-methylphenyl)hydrazine (39943-64-1)

Guidance literature:

Reference yield: 87.0%

2-oxo-propionic acid ethyl ester (617-35-6) + (3-chloro-2-methylphenyl)hydrazine (39943-64-1) → (E)-ethyl 2-(2-(3-chloro-2-methylphenyl)hydrazono)propanoate

Guidance literature:

With acetic acid; at 35 ℃; for 2h;

upstream raw materials:

3-chloro-2-methylbenzenamine

Downstream raw materials:

4-[2-(3-chloro-2-methyl-phenyl)-5-methyl-2H-pyrazol-3-yl]-pyridine

4-[1-(3-chloro-2-methyl-phenyl)-5-methyl-1H-pyrazol-3-yl]-pyridine

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