(3-BroMo-phenylsulfanyl)-acetic acid

Base Information

• Chemical Name: (3-BroMo-phenylsulfanyl)-acetic acid
• CAS No.: 3996-39-2
• Molecular Formula: C8H7BrO2S
• Molecular Weight: 247.112
• Hs Code.: 2930909090
• Mol file: 3996-39-2.mol

Synonyms:<3-Brom-phenylmercapto>-essigsaeure;m-bromophenylthioglycolic acid;(3-diphenylamino)bromobenzene;3-Bromotriphenylamine;m-Bromophenyldiphenylamine;m-bromotriphenylamine;m-bromophenyl-N,N-diphenylamine;(3-bromo-phenylsulfanyl)-acetic acid;N-3-bromophenyl-N,N-diphenylamine;S-(3-Brom-phenyl)-thioglykolsaeure;

Chemical Property of (3-BroMo-phenylsulfanyl)-acetic acid

Chemical Property:

• PSA: 62.60000
• LogP: 2.62580

Purity/Quality:

95% ^*data from raw suppliers

2-(3-Bromophenyl)ethanethioicO-acid 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-BroMo-phenylsulfanyl)-acetic acid

There total 4 articles about (3-BroMo-phenylsulfanyl)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.1%

3-Bromothiophenol (6320-01-0) + chloroacetic acid (79-11-8) → [(3-bromophenyl)sulfanyl]acetic acid (3996-39-2)

Guidance literature:

With sodium hydroxide; In water; at 20 ℃; for 2h; Reflux;

Reference yield:

C8H7BrO2S*C5H5N*Br3H → [(3-bromophenyl)sulfanyl]acetic acid (3996-39-2) + pyridinium hydrobromide perbromide (39416-48-3)

Guidance literature:

In water; acetic acid; at 19.9 - 44.9 ℃; Equilibrium constant;

DOI:10.1002/poc.610080607

Reference yield:

3-Bromothiophenol (6320-01-0) → [(3-bromophenyl)sulfanyl]acetic acid (3996-39-2)

Guidance literature:

With sodium hydroxide; chloroacetic acid;

DOI:10.1021/ja01564a040

upstream raw materials:

3-Bromothiophenol

chloroacetic acid

Downstream raw materials:

1-bromo-3-[(3-bromophenyl)disulfanyl]benzene

3-Bromothiophenol

Glyoxilic acid

m-bromophenylosulfinylacetic acid