[1,1'-Biphenyl]-2-sulfonamide

Base Information

• Chemical Name: [1,1'-Biphenyl]-2-sulfonamide
• CAS No.: 40182-06-7
• Molecular Formula: C12H11NO2S
• Molecular Weight: 233.291
• European Community (EC) Number: 841-176-6
• ChEMBL ID: CHEMBL4091235
• DSSTox Substance ID: DTXSID50494854
• Nikkaji Number: J3.611.419C
• Wikidata: Q82342543
• Mol file: 40182-06-7.mol

Synonyms:[1,1'-Biphenyl]-2-sulfonamide;2-phenylbenzenesulfonamide;40182-06-7;2-phenylbenzene-1-sulfonamide;biphenylsulfonamide;biphenyl sulfonamide;2-biphenylsulfonamide;2-biphenylylsulfonamide;SCHEMBL48885;1,1'-biphenyl-2-sulfonamide;CHEMBL4091235;DTXSID50494854;SBXDENYROQKXBE-UHFFFAOYSA-N;AKOS008106916;CS-0530898;EN300-60307;Z299680984

Chemical Property of [1,1'-Biphenyl]-2-sulfonamide

Chemical Property:

• Melting Point: 121-122 °C(Solv: ethanol (64-17-5); water (7732-18-5))
• Boiling Point: 443.1±38.0 °C(Predicted)
• PSA: 68.54000
• Density: 1.270±0.06 g/cm3(Predicted)
• LogP: 3.78210
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 233.05104977
• Heavy Atom Count: 16
• Complexity: 314

Purity/Quality:

99% ^*data from raw suppliers

2-PHENYLBENZENE-1-SULFONAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=CC=CC=C2S(=O)(=O)N

Technology Process of [1,1'-Biphenyl]-2-sulfonamide

There total 7 articles about [1,1'-Biphenyl]-2-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

iodobenzene (591-50-4) + methyl 2-methyl-2-(phenylsulfonylamido)propionic acid (105441-80-3) → (1,1'-biphenyl)-2-sulphonamide (40182-06-7)

Guidance literature:

iodobenzene; methyl 2-methyl-2-(phenylsulfonylamido)propionic acid; With sodium acetate; palladium diacetate; In acetonitrile; at 100 ℃; for 12h;

With copper(l) iodide; In acetonitrile; at 20 - 100 ℃; for 8h; Solvent; Reagent/catalyst;

DOI:10.1016/j.tet.2016.10.056

Reference yield: 64.0%

[1,1'-biphenyl]-2-diazonium tetrafluoroborate (318-13-8) → (1,1'-biphenyl)-2-sulphonamide (40182-06-7)

Guidance literature:

With sodium metabisulfite; sodium azide; tetrabutylammomium bromide; triphenylphosphine; In water; acetonitrile; at 80 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c8gc03014f

Reference yield:

2'-Amino-N-(3,4-dimethyl-5-isoxazolyl)-[1,1'-biphenyl]-2-sulfonamide (179250-70-5) + 3'-Amino-N-(3,4-dimethyl-5-isoxazolyl)[1,1'-biphenyl]-2-sulfonamide (153623-88-2) → (1,1'-biphenyl)-2-sulphonamide (40182-06-7)

Guidance literature:

In ethyl acetate;

upstream raw materials:

2-phenylbenzenesulfonyl chloride

2'-Amino-N-(3,4-dimethyl-5-isoxazolyl)-[1,1'-biphenyl]-2-sulfonamide

N-(3,4-Dimethyl-5-isoxazolyl)-4'-(2-methylpropyl)-[1,1'-biphenyl]-2-sulfonamide

3'-Amino-N-(3,4-dimethyl-5-isoxazolyl)[1,1'-biphenyl]-2-sulfonamide

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