4-Nitro-N-phenylphthalimide

Base Information

Chemical Name:4-Nitro-N-phenylphthalimide
CAS No.:40392-27-6
Molecular Formula:C14H8N2O4
Molecular Weight:268.229
Hs Code.:2925190090
European Community (EC) Number:926-210-0,651-239-8
DSSTox Substance ID:DTXSID10354041
Nikkaji Number:J443.334C
Wikidata:Q82131968
ChEMBL ID:CHEMBL273605
Mol file:40392-27-6.mol

Synonyms:4-Nitro-N-phenylphthalimide;40392-27-6;5-Nitro-2-phenylisoindoline-1,3-dione;5-nitro-2-phenylisoindole-1,3-dione;5-Nitro-2-phenyl-isoindole-1,3-dione;CHEMBL273605;N-Phenyl-4-nitrophthalimid;5-Nitro-N-phenylphthalimide;Oprea1_288736;Oprea1_853070;SCHEMBL406359;5-nitro-2-phenyl-2,3-dihydro-1H-isoindole-1,3-dione;DTXSID10354041;BDBM50088676;MFCD00191559;STK391465;AKOS000520535;CCG-353873;SB65580;AS-63209;CS-0313539;EU-0033650;FT-0751073;N0574;D91733;5-nitro-2-phenyl-1H-isoindole-1,3(2H)-dione;SR-01000391092;SR-01000391092-1

Suppliers and Price of 4-Nitro-N-phenylphthalimide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Nitro-N-phenylphthalimide
250mg
$ 45.00

TCI Chemical
4-Nitro-N-phenylphthalimide >98.0%(GC)
25g
$ 251.00

Crysdot
5-Nitro-2-phenylisoindoline-1,3-dione 95+%
100g
$ 468.00

Chemenu
5-Nitro-2-phenylisoindoline-1,3-dione 95%
100g
$ 442.00

American Custom Chemicals Corporation
4-NITRO-N-PHENYLPHTHALIMIDE 95.00%
25G
$ 1233.97

Alichem
5-Nitro-2-phenylisoindoline-1,3-dione
100g
$ 487.19

AK Scientific
4-Nitro-N-phenylphthalimide
25g
$ 402.00

Total 14 raw suppliers

Chemical Property of 4-Nitro-N-phenylphthalimide

Chemical Property:

Melting Point:187oC
Boiling Point:471.1oC at 760 mmHg
Flash Point:238.7oC
PSA：83.20000
Density:1.501g/cm3
LogP:2.98360
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:268.04840674
Heavy Atom Count:20
Complexity:439

Purity/Quality:

97% ^*data from raw suppliers

4-Nitro-N-phenylphthalimide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)N2C(=O)C3=C(C2=O)C=C(C=C3)[N+](=O)[O-]

Technology Process of 4-Nitro-N-phenylphthalimide

There total 6 articles about 4-Nitro-N-phenylphthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5466-84-2
4-nitrophthalic anhydride

: 62-53-3
aniline

: 40392-27-6
4-nitro-N-phenylphthalimide

Guidance literature:: With acetic acid; at 120 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.7b03278

Reference yield: 87.0%

: 89-40-7
4-nitrophthalimide

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 40392-27-6
4-nitro-N-phenylphthalimide

Guidance literature:: With [bis(acetoxy)iodo]benzene; at 140 ℃; for 4h;
DOI:10.1021/ja207296y

Reference yield:

: 4727-29-1
phthalanilic acid

: 40392-27-6
4-nitro-N-phenylphthalimide

Guidance literature:: Multi-step reaction with 2 steps

1: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; potassium carbonate; 1-methyl-pyrrolidin-2-one; water / 6 h / 150 °C / Schlenk technique; Inert atmosphere

2: acetic acid / 120 °C / Inert atmosphere

With 1-methyl-pyrrolidin-2-one; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; water; potassium carbonate; acetic acid;
DOI:10.1021/acs.orglett.7b03278