(1,3-Benzodioxol-5-yl)hydrazine hydrochloride, 3,4-(Methylenedioxy)phenylhydrazine hydrochloride

Base Information

Chemical Name:(1,3-Benzodioxol-5-yl)hydrazine hydrochloride, 3,4-(Methylenedioxy)phenylhydrazine hydrochloride
CAS No.:40483-63-4
Molecular Formula:C7H8N2O2.ClH
Molecular Weight:188.614
Hs Code.:2934999090
Mol file:40483-63-4.mol

Synonyms:1,3-Benzodioxol-5-ylhydrazine hydrochloride;Benzo[1,3]-dioxol-5-yl-hydrazine hydrochloride;3,4-(Methylenedioxy)phenylhydrazine hydrochloride;1-(1,3-Benzodioxol-5-yl)hydrazine hydrochloride;2H-1,3-benzodioxol-5-ylhydrazine hydrochloride;benzo[d][1,3]dioxol-5-ylhydrazine hydrochloride;

Suppliers and Price of (1,3-Benzodioxol-5-yl)hydrazine hydrochloride, 3,4-(Methylenedioxy)phenylhydrazine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Hydrazino-1,3-benzodioxoleHydrochloride
500mg
$ 220.00

ChemBridge Corporation
1,3-benzodioxol-5-ylhydrazinehydrochloride 95%
1 g
$ 98.00

Total 2 raw suppliers

Chemical Property of (1,3-Benzodioxol-5-yl)hydrazine hydrochloride, 3,4-(Methylenedioxy)phenylhydrazine hydrochloride

Chemical Property:

PSA：56.51000
LogP:2.27620

Purity/Quality:

97% ^*data from raw suppliers

5-Hydrazino-1,3-benzodioxoleHydrochloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1,3-Benzodioxol-5-yl)hydrazine hydrochloride, 3,4-(Methylenedioxy)phenylhydrazine hydrochloride

There total 4 articles about (1,3-Benzodioxol-5-yl)hydrazine hydrochloride, 3,4-(Methylenedioxy)phenylhydrazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 40483-63-4
benzo[d][1,3]dioxol-5-ylhydrazine hydrochloride

Guidance literature:

Reference yield: 78.0%

: 2635-13-4
1,2-(methylenedioxy)-4-bromobenzene

: 40483-63-4
benzo[d][1,3]dioxol-5-ylhydrazine hydrochloride

Guidance literature:: 1,2-(methylenedioxy)-4-bromobenzene; With potassium phosphate; copper(l) iodide; N,N′-bis(2,6-dimethylphenyl)oxalamide; cetyltrimethylammonim bromide; In water; at 80 ℃; for 0.25h; Schlenk technique; Inert atmosphere; Sealed tube;

With hydrazine hydrate; In water; at 80 ℃; Inert atmosphere; Schlenk technique; Sealed tube;

With hydrogenchloride; In water; pH=3 - 4; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1002/cjoc.201800326

Reference yield: 70.0%

: 14268-66-7
benzo[1,3]dioxolo-5-ylamine

: 40483-63-4
benzo[d][1,3]dioxol-5-ylhydrazine hydrochloride

Guidance literature:: benzo[1,3]dioxolo-5-ylamine; With hydrogenchloride; In water; at 20 ℃; for 1h;

With sodium nitrite; In water; at 0 - 10 ℃; for 4h;

With tin(II) chloride dihdyrate; In water; at 0 - 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2018.02.069