1,2,5-Thiadiazolidine-2,4-dicarboxylic acid, 5-[4-[(2-methyl-4-quinolinyl)methoxy]phenyl]-, 2-(1,1-dimethylethyl) 4-methyl ester, 1,1-dioxide

Base Information

Chemical Name:1,2,5-Thiadiazolidine-2,4-dicarboxylic acid, 5-[4-[(2-methyl-4-quinolinyl)methoxy]phenyl]-, 2-(1,1-dimethylethyl) 4-methyl ester, 1,1-dioxide
CAS No.:409108-11-8
Molecular Formula:C₂₆H₂₉N₃O₇S
Molecular Weight:527.598
Hs Code.:
Mol file:409108-11-8.mol

1,2,5-Thiadiazolidine-2,4-dicarboxylic acid,
5-[4-[(2-methyl-4-quinolinyl)methoxy]phenyl]-, 2-(1,1-dimethylethyl)
4-methyl ester, 1,1-dioxide

Synonyms:

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Chemical Property of 1,2,5-Thiadiazolidine-2,4-dicarboxylic acid, 5-[4-[(2-methyl-4-quinolinyl)methoxy]phenyl]-, 2-(1,1-dimethylethyl) 4-methyl ester, 1,1-dioxide

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Technology Process of 1,2,5-Thiadiazolidine-2,4-dicarboxylic acid, 5-[4-[(2-methyl-4-quinolinyl)methoxy]phenyl]-, 2-(1,1-dimethylethyl) 4-methyl ester, 1,1-dioxide

There total 6 articles about 1,2,5-Thiadiazolidine-2,4-dicarboxylic acid, 5-[4-[(2-methyl-4-quinolinyl)methoxy]phenyl]-, 2-(1,1-dimethylethyl) 4-methyl ester, 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 409108-10-7
5-(4-hydroxy-phenyl)-1,1-dioxo-1λ⁶-[1,2,5]thiadiazolidine-2,4-dicarboxylic acid 2-tert-butyl ester 4-methyl ester

: 288399-19-9
4-(chloromethyl)-2-methylquinoline

: 409108-11-8
5-[4-(2-methyl-quinolin-4-ylmethoxy)-phenyl]-1,1-dioxo-1λ⁶-[1,2,5]thiadiazolidine-2,4-dicarboxylic acid 2-tert-butyl ester 4-methyl ester

Guidance literature:: With potassium carbonate; In acetonitrile;
DOI:10.1016/j.bmcl.2005.10.078

Reference yield:

: 409108-08-3
1,1-dioxo-1λ⁶-[1,2,5]thiadiazolidine-2,4-dicarboxylic acid 2-tert-butyl ester 4-methyl ester

: 409108-11-8
5-[4-(2-methyl-quinolin-4-ylmethoxy)-phenyl]-1,1-dioxo-1λ⁶-[1,2,5]thiadiazolidine-2,4-dicarboxylic acid 2-tert-butyl ester 4-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 20 percent / Cu(OAc)2; Et₃N / CH₂Cl₂

2: H₂ / Pd(OH)2 / methanol

3: 33 percent / K₂CO₃ / acetonitrile

With copper diacetate; hydrogen; potassium carbonate; triethylamine; palladium dihydroxide; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2005.10.078

Reference yield:

: 409108-07-2
5-benzyl-1,1-dioxo-1λ⁶-[1,2,5]thiadiazolidine-2,4-dicarboxylic acid 2-tert-butyl ester 4-methyl ester

: 409108-11-8
5-[4-(2-methyl-quinolin-4-ylmethoxy)-phenyl]-1,1-dioxo-1λ⁶-[1,2,5]thiadiazolidine-2,4-dicarboxylic acid 2-tert-butyl ester 4-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 26 percent / H₂ / Pd(OH)2 / methanol

2: 20 percent / Cu(OAc)2; Et₃N / CH₂Cl₂

3: H₂ / Pd(OH)2 / methanol

4: 33 percent / K₂CO₃ / acetonitrile

With copper diacetate; hydrogen; potassium carbonate; triethylamine; palladium dihydroxide; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2005.10.078