3-Benzyloxy-4-methoxybenzoyl chloride

Base Information

Chemical Name:3-Benzyloxy-4-methoxybenzoyl chloride
CAS No.:41222-60-0
Molecular Formula:C15H13ClO3
Molecular Weight:276.719
Hs Code.:
DSSTox Substance ID:DTXSID90450191
Nikkaji Number:J2.577.642I
Wikidata:Q82269792
Mol file:41222-60-0.mol

Synonyms:3-benzyloxy-4-methoxybenzoyl chloride;41222-60-0;3-(benzyloxy)-4-methoxybenzoyl chloride;4-methoxy-3-phenylmethoxybenzoyl chloride;SCHEMBL184987;DTXSID90450191;IXCKJOOGPMRIDP-UHFFFAOYSA-N;3-benzyloxy4-methoxy-benzoyl chloride;AKOS025131056;3-benzyloxy-4-methoxy-benzoyl chloride;3-benzyloxy-4-methoxy benzoic acid chloride;3-(Benzyloxy)-4-methoxybenzoic acid chloride

Suppliers and Price of 3-Benzyloxy-4-methoxybenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Benzyloxy-4-methoxybenzoyl chloride

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:276.0553220
Heavy Atom Count:19
Complexity:289

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C(=O)Cl)OCC2=CC=CC=C2

Technology Process of 3-Benzyloxy-4-methoxybenzoyl chloride

There total 6 articles about 3-Benzyloxy-4-methoxybenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 58452-00-9
3-benzyloxy-4-methoxybenzoic acid

: 41222-60-0
3-benzyloxy-4-methoxybenzoyl chloride

Guidance literature:: With thionyl chloride; for 2h; Heating / reflux;

Reference yield:

: 6346-05-0
3-benzyloxy-4-methoxybenzaldehyde

: 41222-60-0
3-benzyloxy-4-methoxybenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / sodium chlorite; sulfamic acid; acetic acid / H₂O / 1 h / 20 °C

2: 94 percent / thionyl chloride / toluene / 6 h / 100 °C

With sodium chlorite; thionyl chloride; aminosulfonic acid; acetic acid; In water; toluene;
DOI:10.1016/j.bmc.2006.08.026

Reference yield:

: 621-59-0
isovanillin

: 41222-60-0
3-benzyloxy-4-methoxybenzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / K₂CO₃; KI / dimethylformamide / 22 h / 65 °C

2: 93 percent / sodium chlorite; sulfamic acid; acetic acid / H₂O / 1 h / 20 °C

3: 94 percent / thionyl chloride / toluene / 6 h / 100 °C

With sodium chlorite; thionyl chloride; aminosulfonic acid; potassium carbonate; acetic acid; potassium iodide; In water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2006.08.026