2,6,10-Tridecatrien-1-ol, 13-(3,3-dimethyloxiranyl)-3,7,11-trimethyl-, (2E,6E,10E)-

Base Information

Chemical Name:2,6,10-Tridecatrien-1-ol, 13-(3,3-dimethyloxiranyl)-3,7,11-trimethyl-, (2E,6E,10E)-
CAS No.:41370-60-9
Molecular Formula:C20H34O2
Molecular Weight:306.489
Hs Code.:
Mol file:41370-60-9.mol

Synonyms:

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Chemical Property of 2,6,10-Tridecatrien-1-ol, 13-(3,3-dimethyloxiranyl)-3,7,11-trimethyl-, (2E,6E,10E)-

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2,6,10-Tridecatrien-1-ol, 13-(3,3-dimethyloxiranyl)-3,7,11-trimethyl-, (2E,6E,10E)-

There total 1 articles about 2,6,10-Tridecatrien-1-ol, 13-(3,3-dimethyloxiranyl)-3,7,11-trimethyl-, (2E,6E,10E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5389-87-7
1-chloro-3,7-dimethylocta-2,6-diene

: 41370-60-9
(2E,6E,10E)-13-(3,3-dimethyloxiran-2-yl)-3,7,11-trimethyltrideca-2,6,10-trien-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 1) lithium biphenylide, barium iodide / 1) THF, -78 deg C, 30 min, 2) THF, a) -78 deg C, 1.5 h, b) room temperature, 16 h

2: 95 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 16 h / 23 °C

3: 100 percent / pyridine / 3 h / 23 °C

4: 1) N-bromosuccinimide, 2) potassium carbonate / 1) THF, H₂O, 0 deg C, 1 h, 2) methanol, 23 deg C, 2 h

With pyridine; N-Bromosuccinimide; lithium biphenylide; barium(II) iodide; tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)79008-3

Reference yield:

: 41370-60-9
(2E,6E,10E)-13-(3,3-dimethyloxiran-2-yl)-3,7,11-trimethyltrideca-2,6,10-trien-1-ol

: (4E,8E,12E)-14-[2-Hydroxy-3,4-dimethyl-5-(tetrahydro-pyran-2-yloxy)-phenyl]-4,8,12-trimethyl-tetradeca-4,8,12-trienoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: C₅H₅N

2: 78 percent / HIO₄*2H₂O / diethyl ether

3: Jones reagent / acetone

4: 98 percent / bis(dibenylideneacetone)palladium⁽⁰⁾, LiCl / dimethylformamide

5: 60 percent / CsF, HMPA

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; jones reagent; periodic acid; cesium fluoride; lithium chloride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In diethyl ether; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0040-4039(96)00127-X

Reference yield:

: 41370-60-9
(2E,6E,10E)-13-(3,3-dimethyloxiran-2-yl)-3,7,11-trimethyltrideca-2,6,10-trien-1-ol

: 201004-67-3
(4E,8E,12E)-14-[2-Acetoxy-3,4-dimethyl-5-(tetrahydro-pyran-2-yloxy)-phenyl]-4,8,12-trimethyl-tetradeca-4,8,12-trienoic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: C₅H₅N

2: 78 percent / HIO₄*2H₂O / diethyl ether

3: Jones reagent / acetone

4: 98 percent / bis(dibenylideneacetone)palladium⁽⁰⁾, LiCl / dimethylformamide

5: 60 percent / CsF, HMPA

6: 89 percent / C₅H₅N

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; jones reagent; periodic acid; cesium fluoride; lithium chloride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In diethyl ether; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0040-4039(96)00127-X