1H-1,4-Benzodiazepine, 2,3,4,5-tetrahydro-1-methyl-

Base Information

Chemical Name:1H-1,4-Benzodiazepine, 2,3,4,5-tetrahydro-1-methyl-
CAS No.:4141-14-4
Molecular Formula:C10H14N2
Molecular Weight:162.235
Hs Code.:
Mol file:4141-14-4.mol

Synonyms:2,3,4,5-Tetrahydro-1H-1,4-benzodiazepin;1-methyl-2,3,4,5-tetrahydro-1,4-benzodiazepin;1-Methyl-1,2,3,4,5-pentahydro-1,4-benzodiazepin;1-Methyl-2,3,4,5-tetrahydro-1H-benzo[e][1,4]diazepine;

Suppliers and Price of 1H-1,4-Benzodiazepine, 2,3,4,5-tetrahydro-1-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-methyl-2,3,4,5-tetrahydro-1H-1,4-benzodiazepine
10mg
$ 45.00

AK Scientific
1-Methyl-2,3,4,5-tetrahydro-1H-1,4-benzodiazepine
10g
$ 2665.00

Total 4 raw suppliers

Chemical Property of 1H-1,4-Benzodiazepine, 2,3,4,5-tetrahydro-1-methyl-

Chemical Property:

PSA：15.27000
LogP:1.61980

Purity/Quality:

95% ^*data from raw suppliers

1-methyl-2,3,4,5-tetrahydro-1H-1,4-benzodiazepine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H-1,4-Benzodiazepine, 2,3,4,5-tetrahydro-1-methyl-

There total 4 articles about 1H-1,4-Benzodiazepine, 2,3,4,5-tetrahydro-1-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl 1-methyl-1,2,3,5-tetrahydro-4H-benzo[e][1,4]diazepine-4-carboxylate

: 4141-14-4
1-methyl-2,3,4,5-tetrahydro-1H-benzo[e][1,4]diazepine

Guidance literature:: With trifluoroacetic acid; for 0.333333h;

Reference yield:

: 5946-39-4
2,3,4,5-tetrahydro-1H-benzo[e][1,4]diazepine

: 4141-14-4
1-methyl-2,3,4,5-tetrahydro-1H-benzo[e][1,4]diazepine

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 0.5 h / 20 °C

2: acetic acid / methanol; water / 0.17 h / 20 °C

3: trifluoroacetic acid / 0.33 h

With acetic acid; trifluoroacetic acid; In methanol; dichloromethane; water;

Reference yield:

: 195983-63-2
2,3,4,5-Tetrahydro-4-[(1,1-dimethylethoxy)-carbonyl]-1H-1,4-benzodiazepine

: 4141-14-4
1-methyl-2,3,4,5-tetrahydro-1H-benzo[e][1,4]diazepine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / methanol; water / 0.17 h / 20 °C

2: trifluoroacetic acid / 0.33 h

With acetic acid; trifluoroacetic acid; In methanol; water;