1,12-Bis(diphenylphosphino)dodecane

Base Information

Chemical Name:1,12-Bis(diphenylphosphino)dodecane
CAS No.:41625-32-5
Molecular Formula:C36H44P2
Molecular Weight:538.693
Hs Code.:
DSSTox Substance ID:DTXSID00514238
Nikkaji Number:J1.282.920E
Wikidata:Q82374439

Synonyms:1,12-Bis(diphenylphosphino)dodecane;41625-32-5;DTXSID00514238;BJFFDMZPLFWJSR-UHFFFAOYSA-N;(C6H5)2P(CH2)12P(C6H5)2;(Dodecane-1,12-diyl)bis(diphenylphosphane)

Suppliers and Price of 1,12-Bis(diphenylphosphino)dodecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 1,12-Bis(diphenylphosphino)dodecane

Chemical Property:

Melting Point:66-69 °C
Boiling Point:623.9±28.0 °C(Predicted)
PSA：27.18000
LogP:9.15320
XLogP3:10.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:17
Exact Mass:538.29182540
Heavy Atom Count:38
Complexity:466

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(CCCCCCCCCCCCP(C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 1,12-Bis(diphenylphosphino)dodecane

There total 1 articles about 1,12-Bis(diphenylphosphino)dodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 3344-70-5
1,12-dibromododecane

: 15475-27-1,4346-39-8
potassium diphenylphosphine

: 41625-32-5
1,12-bis(diphenylphosphino)dodecane

Guidance literature:: In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1039/b301874a DOI:10.1021/ma050561g

Reference yield: 57.0%

: trans,trans-(C₆F₅)((p-tolyl)3P)2Pt(CC)3Pt(P(p-tolyl)3)2(C₆F₅)

: 41625-32-5
1,12-bis(diphenylphosphino)dodecane

: 820224-96-2
trans,trans-(C₆F₅)((phenyl)2P(CH₂)12P(phenyl)2)Pt(CC)3Pt((phenyl)2P(CH₂)12P(phenyl)2)(C₆F₅)

Guidance literature:: In tetrahydrofuran; monitoring by NMR;
DOI:10.1021/om0493558

Reference yield: 44.0%

: 108-86-1,52753-63-6
bromobenzene

: 41625-32-5
1,12-bis(diphenylphosphino)dodecane

: 22884-33-9
1,12-bis(triphenylphosphonium)dodecane dibromide

Guidance literature:: With nickel dibromide; In 1,2-dimethoxyethane; at 80 ℃; for 4h; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.ica.2020.119904