2,2,3-Trimethyl-3-butenoic acid

Base Information

• Chemical Name: 2,2,3-Trimethyl-3-butenoic acid
• CAS No.: 4168-01-8
• Molecular Formula: C7H12O2
• Molecular Weight: 128.171
• Hs Code.: 2916190090
• Mol file: 4168-01-8.mol

Synonyms:2,2,3-trimethyl-but-3-enoic acid;2,2,3-Trimethyl-but-3-ensaeure;2,2,3-Trimethyl-3-butenoic acid;

Chemical Property of 2,2,3-Trimethyl-3-butenoic acid

Chemical Property:

• PSA: 37.30000
• LogP: 1.67330

Purity/Quality:

95% ^*data from raw suppliers

2,2,3-Trimethylbut-3-enoicacid 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2,3-Trimethyl-3-butenoic acid

There total 23 articles about 2,2,3-Trimethyl-3-butenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2,2,3-trimethyl-3-butensaeure-aethylester (35293-39-1) → 2,2,3-trimethyl-3-butenoic acid (4168-01-8)

Guidance literature:

With potassium hydroxide; In methanol; water; for 17h; Heating;

DOI:10.1002/hlca.19840670110

Reference yield: 84.0%

methyl 2,2,3-trimethylbut-3-enoate (1727-59-9) → 2,2,3-trimethyl-3-butenoic acid (4168-01-8)

Guidance literature:

With lithium hydroxide; water; In ethanol; Ambient temperature;

DOI:10.1055/s-1998-1782

Reference yield: 81.0%

ethyl 3-chloro-2,2,3-trimethylbutyrate (220264-25-5) → 2,2,3-trimethyl-3-butenoic acid (4168-01-8)

Guidance literature:

With potassium hydroxide; In ethanol; for 2h; Heating;

DOI:10.1021/ja983047h

upstream raw materials:

2,3-Dimethyl-2-butene

carbonyl cyanide

2,2,3-trimethyl-3-butenenitrile

2,2,3-trimethyl-3-butensaeure-aethylester

Downstream raw materials:

3-methyl-butan-2-one

hydroxy-trimethyl-succinic acid

C₂₁H₃₁N₃O₆

C₁₃H₁₇NO₂