4-ethylbenzenediazonium Chloride

Base Information

• Chemical Name: 4-ethylbenzenediazonium Chloride
• CAS No.: 41888-23-7
• Molecular Formula: C8H9N2.Cl
• Molecular Weight: 168.626
• DSSTox Substance ID: DTXSID60450789
• Mol file: 41888-23-7.mol

Synonyms:4-ethylbenzenediazonium Chloride;41888-23-7;AGN-PC-0NDZDG;DTXSID60450789

Chemical Property of 4-ethylbenzenediazonium Chloride

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 168.0454260
• Heavy Atom Count: 11
• Complexity: 137

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC1=CC=C(C=C1)[N+]#N.[Cl-]

Technology Process of 4-ethylbenzenediazonium Chloride

There total 1 articles about 4-ethylbenzenediazonium Chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-aminoethylbenzene (589-16-2) → 4-ethylphenyldiazonium chloride (41888-23-7)

Guidance literature:

With hydrogenchloride; sodium nitrite;

Reference yield: 86.0%

4-ethylphenyldiazonium chloride (41888-23-7) + 11,23-di-tert-butylcalix<4>arene-25,26,27,28-tetrol (137571-15-4) → 25,26,27,28-tetrahydroxy-11,23-di-(tert-butyl)-5,17-(4-ethylphenylazo)calix[4]arene (1446482-14-9)

Guidance literature:

With sodium acetate; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 0 ℃; for 10h;

DOI:10.1016/j.tet.2013.06.018

Reference yield: 78.0%

4-ethylphenyldiazonium chloride (41888-23-7) + Sodium; [6,6-dimethyl-4-oxo-dihydro-pyran-(3Z)-ylidene]-methanolate → 2,2-dimethyl-5-[(4-ethyl-phenyl)hydrazono]-tetrahydro-pyran-4-one

Guidance literature:

In water; at -5 - 0 ℃; for 1h;

DOI:10.1016/S0968-0896(02)00176-1

upstream raw materials:

4-aminoethylbenzene

Downstream raw materials:

9-[(4-Ethyl-phenyl)-hydrazono]-6-methyl-4-oxo-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidine-3-carboxylic acid

1-[5-(4-Ethyl-phenyl)-thiophen-2-yl]-ethanone oxime

1-[5-(4-Ethyl-phenyl)-thiophen-2-yl]-ethanone O-methyl-oxime

1-[5-(4-Ethyl-phenyl)-thiophen-2-yl]-ethanone O-ethyl-oxime