3,4,5-Trimethoxythiobenzamide

Base Information

Chemical Name:3,4,5-Trimethoxythiobenzamide
CAS No.:60987-94-2
Molecular Formula:C10H13NO3S
Molecular Weight:227.28
Hs Code.:2930909090
DSSTox Substance ID:DTXSID60209835
Nikkaji Number:J149.183K
Mol file:60987-94-2.mol

Synonyms:3,4,5-Trimethoxythiobenzamide;3,4,5-Trimethoxybenzothioamide;60987-94-2;3,4,5-trimethoxybenzene-1-carbothioamide;BRN 2697326;BENZAMIDE, THIO-3,4,5-TRIMETHOXY-;Benzenecarbothioamide, 3,4,5-trimethoxy-;SCHEMBL2766557;DTXSID60209835;FCQGHVXXICVSIF-UHFFFAOYSA-N;AKOS002669655;LS-27439;EN300-1848249

Suppliers and Price of 3,4,5-Trimethoxythiobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3,4,5-Trimethoxythiobenzamide

Chemical Property:

Vapor Pressure:2.91E-05mmHg at 25°C
Boiling Point:356.5°C at 760 mmHg
Flash Point:169.4°C
PSA：90.34000
Density:1.208g/cm³
LogP:2.06730
XLogP3:0.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:227.06161445
Heavy Atom Count:15
Complexity:211

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=CC(=C1OC)OC)C(=S)N

Technology Process of 3,4,5-Trimethoxythiobenzamide

There total 6 articles about 3,4,5-Trimethoxythiobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3086-62-2
3,4,5-trimethoxybenzamide

: 60987-94-2
3,4,5-trimethoxythiobenzamide

Guidance literature:: With diphosphorus pentasulfide; sodium hydroxide; In water; benzene;

Reference yield:

: 19172-47-5,94367-93-8
Lawessons reagent

: 3086-62-2
3,4,5-trimethoxybenzamide

: 60987-94-2
3,4,5-trimethoxythiobenzamide

Guidance literature:: In toluene;

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 60987-94-2
3,4,5-trimethoxythiobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride, sodium hydroxide / aq. ethanol; H₂O / Ambient temperature

2: acetic anhydride / Heating

3: hydrogen sulphide gas, triethylamine, pyridine / Ambient temperature

With pyridine; sodium hydroxide; hydrogen sulfide; hydroxylamine hydrochloride; acetic anhydride; triethylamine; In ethanol; water;