2,6-DICHLOROTHIOANISOLE

Base Information

• Chemical Name: 2,6-DICHLOROTHIOANISOLE
• CAS No.: 4210-03-1
• Molecular Formula: C7H6Cl2S
• Molecular Weight: 193.09400
• Hs Code.: 2930909090
• Mol file: 4210-03-1.mol

Synonyms:<2,6-Dichlor-phenyl>-methyl-sulfid;2,6-dichlorophenyl methyl sulphide;

Chemical Property of 2,6-DICHLOROTHIOANISOLE

Chemical Property:

• Boiling Point: 230.1±30.0 °C(Predicted)
• PSA: 25.30000
• Density: 1.35±0.1 g/cm3(Predicted)
• LogP: 3.71530

Purity/Quality:

95% ^*data from raw suppliers

2,6-Dichlorothioanisole 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-DICHLOROTHIOANISOLE

There total 4 articles about 2,6-DICHLOROTHIOANISOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-dichloro-2-thiocyanatobenzene (4148-89-4) → 2,6-dichlorophenyl methyl sulphide (4210-03-1)

Guidance literature:

Multi-step reaction with 3 steps

1: NH₃ / ethanol

2: (i) Cl₂, (ii) /BRN= 956570/

3: 150 - 170 °C

With ammonia; In ethanol;

DOI:10.1016/S0040-4020(01)98339-5

Reference yield:

2,6-Dichloroaniline (608-31-1) → 2,6-dichlorophenyl methyl sulphide (4210-03-1)

Guidance literature:

Multi-step reaction with 4 steps

1: (i) (diazotization), (ii) /BRN= 3561118/, KSCN

2: NH₃ / ethanol

3: (i) Cl₂, (ii) /BRN= 956570/

4: 150 - 170 °C

With ammonia; In ethanol;

DOI:10.1016/S0040-4020(01)98339-5

Reference yield:

Monothiophosphorsaeure-O,O-dimethylester-S-<2,6-dichlor-phenylester> (4184-63-8) → 2,6-dichlorophenyl methyl sulphide (4210-03-1)

Guidance literature:

at 150 - 170 ℃;

DOI:10.1016/S0040-4020(01)98339-5

upstream raw materials:

Monothiophosphorsaeure-O,O-dimethylester-S-<2,6-dichlor-phenylester>

1,3-dichloro-2-thiocyanatobenzene

1,3-dichloro-2-[(2,6-dichlorophenyl)disulfanyl]benzene

2,6-Dichloroaniline

Downstream raw materials:

1,3-dichloro-2-(methylsulfinyl)benzene

<2,6-Dichlor-phenyl>-methyl-sulfon